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Merck
CN

28471-U

Supelco

SLB ®-5 ms 毛细管 GC 色谱柱

L × I.D. 30 m × 0.25 mm, df 0.25 μm

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别名:
GC column, SPB-5, 5% diphenyl, mass spec
UNSPSC代码:
12000000
eCl@ss:
32119290
NACRES:
SB.54

物料

fused silica

质量水平

Agency

Standard Method 6040D
EN 2005/108/EC
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST,610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

管理合规性

FDA LIB 4423

参数

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

β值

250

df

0.25 μm

技术

GC/MS: suitable
gas chromatography (GC): suitable

长度 × 内径

30 m × 0.25 mm

基质活性基团

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

应用

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

色谱柱类型

capillary non-polar

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一般描述

应用 :5% 苯基当量相提供了沸点洗脱顺序,选择性略有增加,尤其是芳香族化合物。低流失特性、惰性和耐久性使其成为环境分析物(如半挥发物、农药、多氯联苯和除草剂)或需要低流失非极性色谱柱的任何地方的选择色谱柱。
USP编码:该色谱柱满足USP G27及G36要求。

  • 粘合和高交联
  • 聚(5% 二苯基/95% 二甲基硅氧烷)硅亚苯基聚合物在极性方面几乎等同于聚(5% 二苯基/95% 二甲基硅氧烷)
温度限制
  • ≤0.32 mm 内径:-60°C 至 340°C(等温)或 360°C(程序化)
  • ≥0.53 mm 内径:-60°C 至 330°C(等温)或 340°C(程序化)

应用


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

其他说明

我们提供各种色谱配件,包括分析进样针。

法律信息

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

应用

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说明
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法规信息

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分析证书(COA)

输入产品批号来搜索 分析证书(COA) 。批号可以在产品标签上"批“ (Lot或Batch)字后找到。

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. How does the SLB-5ms Capillary GC Column differ from our other 5-type columns?

    Many of our other 5-type columns (Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S) incorporate a siloxane polymer (backbone comprised of Si and O atoms only, side groups are either methyl or phenyl). The SLB-5ms column incorporates a silphenylene polymer (backbone comprised of Si and O atoms plus some phenyl groups, side groups are either methyl or phenyl).

  4. What are the benefits of the SLB-5ms Capillary GC Column over other manufacturers’ -5ms columns?

    The SLB-5ms excels in several performance criteria.· Low Bleed. The highly crosslinked silphenylene polymer chemistry reduces column bleed to a very low level, resulting in greater signal-to-noise level, allowing lower detection levels.· Inertness. The proprietary surface deactivation reduces interactions between analytes and the column surface, resulting in sharper peak shapes, allowing lower detection levels.· Durability. With the highest published maximum allowable operating temperature (MAOT) of any -5ms column, SLB-5ms columns are designed for long life.· Consistency. Innovative manufacturing processes result in decreased column variability, ensuring that the next column is as good as the last.

  5. Would you recommend SLB-5ms Capillary GC Columns for all applications instead of Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S?

    Yes.

  6. Who uses SLB-5ms Capillary GC Columns?

    Any analyst with the need for a non-polar column. Some applications include boiling point separations, GC-MS analyses of semivolatiles, and GC-ECD analyses of pesticides/PCBs. It is estimated that non-polar columns account for 51% of the worldwide column market.

  7. What if my method does not allow me to change to SLB-5ms Capillary GC Columns?

    These methods typically specify a 5-type column (DB-5 or equivalent). The SLB-5ms satisfies that requirement.

  8. How do I find price and availability?

    There are several ways to find pricing and availability for our products. Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers.

  9. What is the Department of Transportation shipping information for this product?

    Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

  10. My question is not addressed here, how can I contact Technical Service for assistance?

    Ask a Scientist here.

Tommy W McGaha et al.
PloS one, 10(3), e0118904-e0118904 (2015-03-19)
The suite of pheromones that promote communal oviposition by Simulium vittatum, a North American black fly species, was identified and characterized using gas chromatography-mass spectrometry, electrophysiological, and behavioral bioassays. Behavioral assays demonstrated that communal oviposition was induced by egg-derived compounds
Chemical Characterization of Three Accessions of Brassica juncea L. Extracts from Different Plant Tissues
Oulad El Majdoub Y, et al.
Molecules (Basel), 25(22), 5421-5421 (2020)
Lorenzo Cucinotta et al.
Journal of chromatography. A, 1655, 462473-462473 (2021-09-01)
The use of IRMS as a GC detector has a history going back decades, however the critical issue of wrong δ13C measurements resulting from impure peaks has been often underestimated. To this regard, multidimensional separation techniques are effective tools to
Sophie Duclos et al.
Proteomics, 11(5), 854-864 (2011-02-01)
The essential roles of the endovacuolar system in health and disease call for the development of new tools allowing a better understanding of the complex molecular machinery involved in endocytic processes. We took advantage of the floating properties of small
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction

商品

Resolving by Mass

GC Analysis of Neroli Essential Oil on SLB®-5ms

质量解析

Learn more about how the thermal desorption technique is applied for terpene identification, profiling, odor measurement, industrial hygiene, and environmental emissions.

实验方案

GC Analysis of PBDE Flame-Retardant Compounds

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

示例显示了使用SLB-5ms GC色谱柱的苯丙胺的MSTFA/MSTFA-d9衍生化如何在质谱图和色谱图中提供有价值的信息。

Example displays how MSTFA/MSTFA-d9 derivatization of amphetamine provides valuable information in mass spectra and chromatograms using SLB-5ms GC column.

查看所有结果

Chromatograms

suitable for GCsuitable for GCsuitable for GC, application for SPMEsuitable for GC, application for SPME展开

我们的科学家团队拥有各种研究领域经验,包括生命科学、材料科学、化学合成、色谱、分析及许多其他领域.

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