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Merck
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主要文件

28471-U

Supelco

SLB ®-5 ms 毛细管 GC 色谱柱

L × I.D. 30 m × 0.25 mm, df 0.25 μm

别名:

气相色谱柱,SPB-5,5%二苯基,质谱检测

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1 KIT
¥5,282.92

About This Item

UNSPSC代码:
41115710
eCl@ss:
32119290
NACRES:
SB.54

¥5,282.92


请联系客服了解存货情况
新价格,新优惠!

物料

fused silica

质量水平

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

管理合规性

FDA LIB 4423

参数

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

β值

250

df

0.25 μm

技术

GC/MS: suitable
gas chromatography (GC): suitable

长度 × 内径

30 m × 0.25 mm

基质活性基团

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

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RAB0469RAB0473RAB0467
Gene Information

mouse ... Timp1(21857)

Gene Information

mouse ... Timp1(21857)

Gene Information

mouse ... Timp2(21858)

Gene Information

human ... TIMP1(7076)

species reactivity

mouse

species reactivity

mouse

species reactivity

mouse

species reactivity

human

assay range

inter-assay cv: <12%
intra-assay cv: <10%
sensitivity: 3 pg/mL
standard curve range: 1.37-1000 pg/mL

assay range

inter-assay cv: <12%
intra-assay cv: <10%
sensitivity: 3 pg/mL
standard curve range: 1.37-1000 pg/mL

assay range

inter-assay cv: <12%
intra-assay cv: <10%
sensitivity: 80 pg/mL
standard curve range: 0.0823-60 ng/mL

assay range

inter-assay cv: <12%
intra-assay cv: <10%
sensitivity: 30 pg/mL
standard curve range: 24.69-18000 pg/mL

input

sample type cell culture supernatant(s)
sample type plasma
sample type serum

input

sample type cell lysate
sample type tissue lysate

input

sample type cell culture supernatant(s)
sample type plasma
sample type serum

input

sample type tissue lysate
sample type cell lysate

technique(s)

ELISA: suitable, capture ELISA: suitable

technique(s)

ELISA: suitable, capture ELISA: suitable

technique(s)

ELISA: suitable, capture ELISA: suitable

technique(s)

ELISA: suitable, capture ELISA: suitable

storage temp.

−20°C

storage temp.

−20°C

storage temp.

−20°C

storage temp.

−20°C

一般描述

应用 :5% 苯基当量相提供了沸点洗脱顺序,选择性略有增加,尤其是芳香族化合物。低流失特性、惰性和耐久性使其成为环境分析物(如半挥发物、农药、多氯联苯和除草剂)或需要低流失非极性色谱柱的任何地方的选择色谱柱。
USP编码:该色谱柱满足USP G27及G36要求。

  • 粘合和高交联
  • 聚(5% 二苯基/95% 二甲基硅氧烷)硅亚苯基聚合物在极性方面几乎等同于聚(5% 二苯基/95% 二甲基硅氧烷)
温度限制
  • ≤0.32 mm 内径:-60°C 至 340°C(等温)或 360°C(程序化)
  • ≥0.53 mm 内径:-60°C 至 330°C(等温)或 340°C(程序化)

应用


  • 通过气相色谱-串联质谱法测定台湾青枣中丙雀石、戊康唑和溴丙酯类农药残留。:该研究采用SLB-5ms毛细管气相色谱柱对农产品中农药残留进行分析。该方法具有较高的灵敏度和特异性,突出了色谱柱在复杂样品基质中的有效性(Zhang et al., 2014)。

  • 通过脂肪酸甲酯的气相色谱-质谱分析表征毛细管离子液体柱。:该研究探索了SLB-5ms毛细管气相色谱柱分析脂肪酸甲酯的性能。色谱柱具有优异的分辨率和稳定性,使其成为生化应用中脂质分析的宝贵工具(Zeng et al., 2013)。

其他说明

我们提供各种色谱配件,包括分析进样针。

法律信息

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

应用

产品编号
说明
价格

  • 历史批次信息供参考:

    分析证书(COA)

    Lot/Batch Number

    没有发现合适的版本?

    如果您需要特殊版本,可通过批号或批次号查找具体证书。

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    在文件库中查找您最近购买产品的文档。

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    1. Which document(s) contains shelf-life or expiration date information for a given product?

      If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

    2. How do I get lot-specific information or a Certificate of Analysis?

      The lot specific COA document can be found by entering the lot number above under the "Documents" section.

    3. How does the SLB-5ms Capillary GC Column differ from our other 5-type columns?

      Many of our other 5-type columns (Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S) incorporate a siloxane polymer (backbone comprised of Si and O atoms only, side groups are either methyl or phenyl). The SLB-5ms column incorporates a silphenylene polymer (backbone comprised of Si and O atoms plus some phenyl groups, side groups are either methyl or phenyl).

    4. What are the benefits of the SLB-5ms Capillary GC Column over other manufacturers’ -5ms columns?

      The SLB-5ms excels in several performance criteria.· Low Bleed. The highly crosslinked silphenylene polymer chemistry reduces column bleed to a very low level, resulting in greater signal-to-noise level, allowing lower detection levels.· Inertness. The proprietary surface deactivation reduces interactions between analytes and the column surface, resulting in sharper peak shapes, allowing lower detection levels.· Durability. With the highest published maximum allowable operating temperature (MAOT) of any -5ms column, SLB-5ms columns are designed for long life.· Consistency. Innovative manufacturing processes result in decreased column variability, ensuring that the next column is as good as the last.

    5. Would you recommend SLB-5ms Capillary GC Columns for all applications instead of Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S?

      Yes.

    6. Who uses SLB-5ms Capillary GC Columns?

      Any analyst with the need for a non-polar column. Some applications include boiling point separations, GC-MS analyses of semivolatiles, and GC-ECD analyses of pesticides/PCBs. It is estimated that non-polar columns account for 51% of the worldwide column market.

    7. What if my method does not allow me to change to SLB-5ms Capillary GC Columns?

      These methods typically specify a 5-type column (DB-5 or equivalent). The SLB-5ms satisfies that requirement.

    8. How do I find price and availability?

      There are several ways to find pricing and availability for our products. Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers.

    9. What is the Department of Transportation shipping information for this product?

      Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

    10. My question is not addressed here, how can I contact Technical Service for assistance?

      Ask a Scientist here.

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    Journal of chromatography. A, 1655, 462473-462473 (2021-09-01)
    The use of IRMS as a GC detector has a history going back decades, however the critical issue of wrong δ13C measurements resulting from impure peaks has been often underestimated. To this regard, multidimensional separation techniques are effective tools to
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    示例显示了使用SLB-5ms GC色谱柱的苯丙胺的MSTFA/MSTFA-d9衍生化如何在质谱图和色谱图中提供有价值的信息。

    Example displays how MSTFA/MSTFA-d9 derivatization of amphetamine provides valuable information in mass spectra and chromatograms using SLB-5ms GC column.

    查看所有结果

    Chromatograms

    suitable for GC, application for SPMEsuitable for GCsuitable for GC, application for SPMEsuitable for GC展开

    我们的科学家团队拥有各种研究领域经验,包括生命科学、材料科学、化学合成、色谱、分析及许多其他领域.

    联系客户支持