GC Analysis of LSD (TMS Derivatives) on SLB^®-5ms

技术

gas chromatography (GC): suitable

试验参数

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 150 C (1.50 min), 20 C/min to 300 C (20 min)
inj. temp.: 250 °C
MSD interface: 330 °C
scan range: m/z 45-525
carrier gas: helium, 0.7 mL/min constant
injection: 0.5 μL pulsed splitless, 30 psi. (0.20 min), purge on (1.5 min), purge flow (50.0 mL/min)
liner: 2mm I.D., straight
sample: Derivatized LSD using BSTFA

应用

forensics and toxicology