技术
gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable
试验参数
sample/matrix: white wine spiked with 50 ppb pesticides
SPME fiber: 85 μm polyacrylate (57304)
extraction: immersion, room temp (30 min)
desorption process: 250 °C for 5 min
column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 60 °C (1 min), 15 °C/min to 100 °C, 7 °C/min to 300 °C (1 min)
MSD interface: 325 °C
scan range: SIM
carrier gas: helium, 0.7 mL/min, constant
liner: 0.75 mm I.D. SPME liner
适用性
application for SPME
应用
food and beverages
法律信息
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
Diazinon
Vinclozolin
1-Naphthyl-N-methylcarbamate
Methiocarb, analytical standard
Dichlofluanid
Parathion
Triadimefon
Procymidone
Myclobutanil
Dicofol
Phosalone
Azinphos-methyl
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