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安全信息

28467-U

Supelco

SLB ®-5 ms 毛细管 GC 色谱柱

L × I.D. 30 m × 0.25 mm, df 0.10 μm

别名:

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

UNSPSC代码:
12000000
eCl@ss:
32119290
NACRES:
SB.54

物料

fused silica

质量水平

100

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

管理合规性

FDA LIB 4423

参数

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

β值

625

df

0.10 μm

技术

GC/MS: suitable
gas chromatography (GC): suitable

长度 × 内径

30 m × 0.25 mm

基质活性基团

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

应用

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

色谱柱类型

capillary non-polar

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相关类别

一般描述

应用 ：5% 苯基当量相提供了沸点洗脱顺序，选择性略有增加，尤其是芳香族化合物。低流失特性、惰性和耐久性使其成为环境分析物（如半挥发物、农药、多氯联苯和除草剂）或需要低流失非极性色谱柱的任何地方的选择色谱柱。
USP编码：该色谱柱满足USP G27及G36要求。
相：
  • 粘合和高交联
  • 聚（5% 二苯基/95% 二甲基硅氧烷）硅亚苯基聚合物在极性方面几乎等同于聚（5% 二苯基/95% 二甲基硅氧烷）
温度限制：
  • ≤0.32 mm 内径：-60°C 至 340°C（等温）或 360°C（程序化）
  • ≥0.53 mm 内径：-60°C 至 330°C（等温）或 340°C（程序化）

应用

  • An improved method for cyanide determination in blood using solid-phase microextraction and gas chromatography/mass spectrometry.: This study presents an enhanced method for determining cyanide levels in blood, employing solid-phase microextraction combined with gas chromatography/mass spectrometry. This technique improves sensitivity and accuracy, essential for toxicological and forensic analysis (Frison et al., 2006).
  • Photochemical production of conjugated linoleic acid from soybean oil.: This research explores the photochemical production of conjugated linoleic acid (CLA) from soybean oil. The study utilized gas chromatography for the analysis of CLA, demonstrating an efficient method for producing this valuable compound with potential health benefits (Gangidi & Proctor, 2004).
  • Development of a solid-phase microextraction GC-NPD procedure for the determination of free volatile amines in wastewater and sewage-polluted waters.: This work describes the development of a GC-NPD procedure using solid-phase microextraction for detecting volatile amines in wastewater. This method offers improved detection limits and specificity, which are critical for environmental monitoring and water quality assessment (Abalos et al., 1999).

其他说明

We offer a variety of chromatography accessories including analytical syringes

法律信息

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

法规信息

新产品

Choose from one of the most recent versions:

分析证书(COA)

Lot/Batch Number
291348-07
291348-06
291348-05
291348-04
291348-03

Don't see the Right Version?

If you require a particular version, you can look up a specific certificate by the Lot or Batch number.

Search for a COA

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. How does the SLB™-5ms Capillary GC Column differ from our other 5-type columns?

    Many of our other 5-type columns (Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S) incorporate a siloxane polymer (backbone comprised of Si and O atoms only, side groups are either methyl or phenyl). The SLB-5ms column incorporates a silphenylene polymer (backbone comprised of Si and O atoms plus some phenyl groups, side groups are either methyl or phenyl).

  4. What are the benefits of the SLB™-5ms Capillary GC Column over other manufacturers’ -5ms columns?

    The SLB-5ms excels in several performance criteria.· Low Bleed. The highly crosslinked silphenylene polymer chemistry reduces column bleed to a very low level, resulting in greater signal-to-noise level, allowing lower detection levels.· Inertness. The proprietary surface deactivation reduces interactions between analytes and the column surface, resulting in sharper peak shapes, allowing lower detection levels.· Durability. With the highest published maximum allowable operating temperature (MAOT) of any -5ms column, SLB-5ms columns are designed for long life.· Consistency. Innovative manufacturing processes result in decreased column variability, ensuring that the next column is as good as the last.

  5. Would you recommend SLB™-5ms Capillary GC Columns for all applications instead of Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S?

    Yes.

  6. Who uses SLB™-5ms Capillary GC Columns?

    Any analyst with the need for a non-polar column. Some applications include boiling point separations, GC-MS analyses of semivolatiles, and GC-ECD analyses of pesticides/PCBs. It is estimated that non-polar columns account for 51% of the worldwide column market.

  7. What if my method does not allow me to change to SLB™-5ms Capillary GC Columns?

    These methods typically specify a 5-type column (DB-5 or equivalent). The SLB-5ms satisfies that requirement.

  8. How do I find price and availability?

    There are several ways to find pricing and availability for our products. Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers.

  9. What is the Department of Transportation shipping information for this product?

    Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

  10. My question is not addressed here, how can I contact Technical Service for assistance?

    Ask a Scientist here.

Alessia Arena et al.
Food chemistry, 396, 133721-133721 (2022-07-24)
Phthalic acid esters (PAEs), known as phthalates, have a variety of industrial applications, mainly related to their ability to increase plastic softness,flexibility, and durability. With regard to toxicological aspects, several studies suggest that phthalates would act as endocrine-disrupting chemicals, and
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
Annie Xu Zeng et al.
Analytica chimica acta, 803, 166-173 (2013-11-13)
Due to their distinct chemical properties, the application of ionic liquid (IL) compounds as gas chromatography (GC) stationary phases offer unique GC separation especially in the analysis of geometric and positional fatty acid methyl ester (FAME) isomers. Elution behaviour of
Sophie Duclos et al.
Proteomics, 11(5), 854-864 (2011-02-01)
The essential roles of the endovacuolar system in health and disease call for the development of new tools allowing a better understanding of the complex molecular machinery involved in endocytic processes. We took advantage of the floating properties of small
Cedric F A Floquet et al.
Talanta, 150, 240-252 (2016-02-04)
Using the carminic acid assay, we determined the concentration of boron in oilfield waters. We investigated the effect of high concentrations of salts and dissolved metals on the assay performance. The influence of temperature, development time, reagent concentration, and water
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