技术
gas chromatography (GC): suitable
试验参数
column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 40 °C (3 min), 15 °C/min to 325 °C (15 min)
inj. temp.: 250 °C
detector: FID, 325 °C
carrier gas: helium, 25 cm/sec constant
injection: 1 μL splitless (1 min)
liner: 4 mm I.D., single taper, unpacked
sample: solvent extracts of septa, dodecane (as an internal standard) added to 100 μg/mL
应用
general analytical
法律信息
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany
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