技术
gas chromatography (GC): suitable
试验参数
column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 50 °C, 3 °C/min to 250 °C (5 min)
inj. temp.: 250 °C
detector: FID, 300 °C
carrier gas: helium, 30 cm/sec, constant
injection: Wet needle, 100:1 split
sample: cold pressed bergamot oil
应用
flavors and fragrances
分析说明
Bergamot oil is used in cosmetic preparations such as perfumes and lotions, and in flavor formulations included in various candies and beverages. The cold-pressed oil is obtained by the rasping of the peel of the citrus bergamia fruit. The oil is commonly treated prior to use to remove furocoumarins and bergapten, which have the potential to cause advserse skin reactions. In addition, terpenes are often reduced or removed to enhance the desirable top-notes of the oil (1). This application illustrates the analysis of a sample of cold-pressed bergamot oil on the SLB-5ms.
法律信息
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
Tricyclene
α-Thujene
α-Pinene
Camphene
Sabinene
(+)-β-Pinene
6-Methyl-5-hepten-2-one
Myrcene
Octanal
α-Phellandrene
Hexyl acetate
α-Terpinene
p-Cymene
Dipentene
(Z)-beta-Ocimene
(E)-beta-Ocimene
γ-Terpinene
cis-Sabinene hydrate
Terpinolene
Linalool
Nonanal
n-Heptyl acetate
4,8-Dimethyl-1,3-(E),7-nonatriene
(+)-cis-Limonene 1,2-epoxide
(−)-trans-Limonene 1,2-epoxide
Camphor
CitronellaI
(+)-Terpinen-4-ol
α-Terpineol
Decanal
Octyl acetate
cis-3,7-Dimethyl-2,6-octadien-1-ol
Citronellol
Neral
Linalyl acetate
Geranial
Isobornyl acetate
Perillaldehyde
Undecanal
Nonyl acetate
Methyl geranate
Linalyl propionate
delta-Elemene
alpha-Terpinyl acetate + Citronellyl acetate
Neryl acetate
Geranyl acetate
(−)-β-Elemene
n-Decyl acetate
cis-alpha-Bergamotene
(E)-Caryophyllene
trans-α-Bergamotene
(Z)-beta-Farnesene
(E)-beta-Farnesene
α-Humulene
β-Santalene
α-Curcumene
Germacrene D
trans-beta-Bergamotene
Bicyclogermacrene
(Z)-alpha-Bisabolene
(E,E)-alpha-Farnesene
β-Bisabolene
(Z)-gamma-Bisabolene
(+)-δ-Cadinene
beta-Sesquiphellandrene
(E)-gamma-Bisabolene
(E)-alpha-Bisabolene
cis-Sesquisabinene hydrate
(E)-Nerolidol
Spathulenol
Campherenol
epi-beta-Bisabolol
α-Bisabolol
(+)-Nootkatone
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