反应适用性
reagent type: catalyst
core: palladium
reaction type: Miyaura Borylation Reaction
官能团
phosphine
一般描述
应用
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets
Each kit contains 2 customizable screening sets that include the following components:
- 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
- 4 x 4 mL reaction vials with pre-weighed KOAc
- Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
- 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
- 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
- 4 stir bars for substrate stock solution vials.
- 1 internal standard.
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
特点和优势
- Designed and tested by synthetic chemists.
- Easily run 24-microscale reactions in parallel.
- 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
- Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.
法律信息
试剂盒组分也可单独购买
- 764175P(Cy3) Pd G3, 97%化学品安全说明书
- 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri™, ACS reagent, ≥99.0%化学品安全说明书
- 804274XPhos Pd G4, 95%化学品安全说明书
- 804282SPhos Pd G4化学品安全说明书
- 804290RuPhos Pd G4化学品安全说明书
- 804975DTBPF-Pd-G3化学品安全说明书
- 900349cataCXium Pd G4化学品安全说明书
- 900522Toluene, anhydrous, ZerO2®, 99.8%化学品安全说明书
- 900631Ethylene glycol, anhydrous, ZerO2®, 99.8%化学品安全说明书
- 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8%化学品安全说明书
- 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%化学品安全说明书
- 9006391-Butanol, anhydrous, ZerO2®, 99.8%化学品安全说明书
- 900641Methanol, anhydrous, ZerO2®, 99.8%化学品安全说明书
- 900644Acetonitrile, anhydrous, ZerO2®, 99.8%化学品安全说明书
- 900690N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5%化学品安全说明书
- 221171Pinacol, 98%化学品安全说明书
- 473294Bis(pinacolato)diboron, 99%化学品安全说明书
- 754242Tetrahydroxydiboron, 95%化学品安全说明书
- B34656Biphenyl, ReagentPlus®, 99.5%化学品安全说明书
- Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm化学品安全说明书
- Z742110KitAlysis™ 24-well reaction block replacement film化学品安全说明书
相关产品
警示用语：
Danger
危险分类
Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1 - STOT SE 3
靶器官
Central nervous system, Eyes,Central nervous system, Kidney, Respiratory system
补充剂危害
WGK
WGK 3
闪点(°F)
1.4 °F
闪点(°C)
-17 °C
法规信息
商品
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
实验方案
Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.
相关内容
化学反应的设计和优化是有机合成研究的重要手段，通过改变反应参数，例如催化剂、反应体系pH值、反应溶剂、温度或时间等来节约成本、提高反应的选择性、产物的收率和纯度等
Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.
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