HPLC Analysis of Jacobsen Catalyst Enantiomers on Astec^® CYCLOBOND I 2000 HP-RSP (TEA mobile phase)

技术

HPLC: suitable

试验参数

column: CYCLOBOND I 2000 HP-RSP, 25 cm x 4.6 mm I.D., 5 μm particles (24024AST)
mobile phase: [A] acetonitrile; [B] methanol; [C] acetic acid; [D] triethylamine; (95:5:0.2:0.1, A:B:C:D)
column temp.: 25 °C
flow rate: 1.5 mL/min
detector: UV, 254 nm
injection: 2 μL
sample: 5 mg/mL in methanol

适用性

application for HPLC

应用

chemicals and industrial polymers