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73033AST

Supelco

Astec® CHIRALDEX™ G-TA 毛细管GC色谱柱

L × I.D. 30 m × 0.25 mm, df 0.12 μm

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别名:
GC column, chiral, gamma-dextran
UNSPSC代码:
41115710
NACRES:
SB.54

物料

fused silica

质量水平

100

描述

GC capillary column

包装

pkg of 1 ea

参数

-10-180 °C temperature (isothermal or programmed)

β值

500

df

0.12 μm

技术

gas chromatography (GC): suitable

长度 × 内径

30 m × 0.25 mm

基质活性基团

non-bonded; 2,6-di-O-pentyl-3-trifluoroacetyl derivative of γ-cyclodextrin phase

应用

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
life science and biopharma
personal care
pharmaceutical (small molecule)

色谱柱类型

capillary chiral

分离技术

chiral

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相关类别

一般描述

Astec® CHIRALDEX G-TA 是第 1 组 CSP（表面相互作用，复合衍生物）的首选。该阶段已被证明是制药行业最广泛选择的阶段，特别是在临床试验的各个阶段中手性中间体和药物研究的分析。在没有包含机制的情况下发生分离，并且通常比大多数手性固定相更快且更有效。G-TA 也被用于分离母体药物对映体及其代谢物。G-TA 对含氧分析物的选择性最高，如醇、二醇和多元醇，作为游离醇和酰基衍生物；胺类作为酰基衍生物；氨基醇、卤素（Cl> Br> F）、氨基酸、羟基酸、内酯、呋喃和吡喃。它对卤化物也具有高选择性。

应用

Astec® CHIRALDEX™ G-TA（2，6-二-O-戊基-3-三氟乙酰基-γ-环糊精）衍生的环糊精手性固定相可用于毛细管气相色谱，用于从 7 种外消旋亚磺酸酯中分离四种异构体。将其用于通过分析海洋细菌 Erythrobacter litoralis HTCC2594 的开放阅读框（ORF）鉴定的三种环氧化物水解酶的克隆和表征的实验研究。它还用于 HPLC 和 GC 分析环氧化物的转化过程中，环氧化物水解酶从农杆菌放射杆菌（EchA）的对映选择性（使用易错 PCR 和 DNA 改组）。

化学/物理抗性

温度限制：
  • -10 °C 至 180 °C 等温和程序的

其他说明

我们提供各种色谱配件，包括分析注射器

法律信息

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

应用

产品编号
说明
价格

G005039

GC Analysis of 2-Aminobutane (2-Butylamine) Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005049

GC Analysis of 1-Methyl-3-Phenylpropylamine (4-Phenyl-2-Butylamine) Enantiomers (N-TFA Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005056

GC Analysis of β-Butyrolactone Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005061

GC Analysis of Methionine Methyl Ester Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005064

GC Analysis of 2-Halohydrocarbon Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005067

GC Analysis of Mandelic Acid Methyl Ester Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005093

GC Analysis of 1,2-Alkyldiol Enantiomers (O-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005122

GC Analysis of 2,5-Dimethoxytetrahydrofuran Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005096

GC Analysis of 2-Butanol Enantiomers (O-Acetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005095

GC Analysis of 2-Butanol Enantiomers (O-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005094

GC Analysis of 2-Butanol Enantiomers (Underivatized) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005103

GC Analysis of 5-Amino-1,3,3-Trimethylcyclohexanemethylamine Enantiomers (N-TFA Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005131

GC Analysis of Glycidol Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005102

GC Analysis of Proline Methyl Ester Enantiomers (N-Acetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005101

GC Analysis of Proline Methyl Ester Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-TA, suitable for GC

G005076

GC Analysis of Verbenone Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005098

GC Analysis of Wieland-Miescher Ketone Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005111

GC Analysis of α-Hexachlorocyclohexane (α-HCH) Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G005146

GC Analysis of δ-Decanolactone Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G006117

GC Analysis of Volatile Flavor Compound Enantiomers on Astec® CHIRALDEX™ G-TA, suitable for GC

G006154

GC Analysis of D-Carvone Enantiomer in Caraway Essential Oil on Astec® CHIRALDEX™ G-TA, suitable for GC

G006155

GC Analysis of D-Carvone Enantiomer in Dill Seed Essential Oil on Astec® CHIRALDEX™ G-TA, suitable for GC

G006156

GC Analysis of D & L-Carvone Enantiomers in Caraway Essential Oil (Spiked with L-Carvone Enantiomer) on Astec® CHIRALDEX™ G-TA, suitable for GC

G006157

GC Analysis of D & L-Carvone Enantiomers in Dill Seed Essential Oil (Spiked with L-Carvone Enantiomer) on Astec® CHIRALDEX™ G-TA, suitable for GC

G006158

GC Analysis of D & L-Carvone Enantiomers in Native Spearmint Essential Oil (Spiked with D-Carvone Enantiomer) on Astec® CHIRALDEX™ G-TA, suitable for GC

G006159

GC Analysis of D & L-Carvone Enantiomers in Scotch Spearmint Essential Oil (Spiked with D-Carvone Enantiomer) on Astec® CHIRALDEX™ G-TA, suitable for GC

G006160

GC Analysis of D & L-Carvone Enantiomers on Astec CHIRALDEX™ G-TA, suitable for GC

G006162

GC Analysis of L-Carvone Enantiomer in Scotch Spearmint Essential Oil on Astec® CHIRALDEX™ G-TA, suitable for GC

法规信息

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. How do I find price and availability?

    There are several ways to find pricing and availability for our products. Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers.

  4. What is the Department of Transportation shipping information for this product?

    Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

  5. What is the regeneration procedure for Chiraldex TA columns? 

    The regeneration procedure for ChiraldexTA columns is located in Supelco brochure, T407123 (JCH), A Guide to Using Cyclodextrin Bonded Phases for Chiral Separations by Capillary Gas Chromatography, on pages 8 and 9.  These pages are attached.

  6. My question is not addressed here, how can I contact Technical Service for assistance?

    Ask a Scientist here.

Jung-Hee Woo et al.
Applied microbiology and biotechnology, 76(2), 365-375 (2007-06-02)
Previously, we reported that ten strains belonging to Erythrobacter showed epoxide hydrolase (EHase) activities toward various epoxide substrates. Three genes encoding putative EHases were identified by analyzing open reading frames of Erythrobacter litoralis HTCC2594. Despite low similarities to reported EHases
Bert van Loo et al.
Chemistry & biology, 11(7), 981-990 (2004-07-24)
The enantioselectivity of epoxide hydrolase from Agrobacterium radiobacter (EchA) was improved using error-prone PCR and DNA shuffling. An agar plate assay was used to screen the mutant libraries for activity. Screening for improved enantioselectivity was subsequently done by spectrophotometric progress
The synthesis of enantioenriched a-hydroxy esters
Gu, Xin, et al.
Tetrahedron Asymmetry, 25 (24), 1573-1580 (2014)
Isolation of racemic 2,4-pentanediol and 2,5-hexanediol from commercial mixtures of racemic and meso isomers by way of cyclic sulfites.
Caron, Gaetan; Kazlauskas, R.J.
Tetrahedron Asymmetry, 5 (4), 657-664 (1994)
The asymmetric hydrogenation of 2-phenethylacrylic acid as the key step for the enantioselective synthesis of Citralis Nitrile?
Scrivanti, Alberto, et al.
Tetrahedron Letters, 47 (52), 9261-9265 (2006)
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