24024AST
Astec® CYCLOBOND I 2000 HP-RSP Chiral (5 μm) HPLC Columns
L × I.D. 25 cm × 4.6 mm, HPLC Column
别名:
TM=["CYCLOBOND"] I 2000 HP-RSP手性HPLC色谱柱
产品名称
Astec® CYCLOBOND I 2000 HP-RSP手性HPLC色谱柱, 5 μm particle size, L × I.D. 25 cm × 4.6 mm
material
stainless steel column
product line
Astec®
packaging
pkg of 1 ea
manufacturer/tradename
Astec®
parameter
0-50 °C temperature
172 bar pressure (2500 psi)
technique(s)
HPLC: suitable
LC/MS: suitable
L × I.D.
25 cm × 4.6 mm
matrix
silica particle platform
fully porous particle
matrix active group
cyclodextrin, beta- phase
particle size
5 μm
pore size
100 Å
operating pH
3.5-7
separation technique
chiral
Quality Level
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General description
这种新固定相的设计目的在于开发一种稳定性和重现性良好的键合相，保留时间更短，并具有比 CYCLOBOND I 2000 RSP 更好的选择性。目标完成并超额实现，CYCLOBOND I 2000 HP-RSP 通过增加氢键作用提高了分离能力，为手性筛选提供广泛的手性选择性。它最适合于碱性和中性化合物。
- 键合相：(R,S)-羟丙基改性的 β-环糊精（高效）
Legal Information
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
存储类别
13 - Non Combustible Solids
wgk
WGK 1
flash_point_f
Not applicable
flash_point_c
Not applicable
Indirect photodetection of pregnanolone on a Cyclobond column by high-performance liquid chromatography
Agnus, Benoit, et al.
Journal of Chromatography A, 633 (1), 27-33 (1994)
Rapid high-performance liquid chromatographic separation of barley malt a-amylase on cyclobond columns
Henson, Cynthia A., Stone, Julie M.
Journal of Chromatography A, 469, 361-367 (1989)
Assessment of the complexation degree of camptothecin derivatives and cyclodextrins using spectroscopic and separative methodologies
Foulon, C., et al.
Tetrahedron Asymmetry, 20 (21), 2482-2489 (2009)
Reprint of: Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 968, 40-48 (2014)
High-performance liquid chromatographic enantioseparation of bicalutamide and its related compounds.
Roland Török et al.
Journal of chromatography. A, 1098(1-2), 75-81 (2005-11-30)
Direct high-performance liquid chromatographic methods were developed for the enantioseparation of (R,S)-bicalutamide (1) and its analogs (+/-)-3-chloro-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide (2), (+/-)-N-(4-cyano-3-(trifluoro-methyl)phenyl)-2-methyloxirane-2-carboxamide (3), (+/-)-4-fluorophenylsulfonyl-2-hydroxy-2-methylpropionic acid (4) and (+/-)-3-hydroxy-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide (5). The methods involved the use of a cellulose-based Chiralcel OD-H, macrocyclic glycopeptide-based Chirobiotic T
相关内容
CYCLOBOND is the name given to Astec technology for bonding cyclodextrins to a high purity silica gel through a stable ether linkage.
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