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223689

Sigma-Aldrich

二(氰基苯)二氯化钯(II)

greener alternative

95%

别名:

二(氰基苯)二氯化钯(II), 二氯化钯双（苯甲腈）, 二氯双（苯甲腈）钯, 二氯双（苯甲腈）钯 (II), 二苯甲腈二氯化钯, 双（苯甲腈）二氯化钯 (II), 双（苯腈）二氯化钯, 氯化钯(II)双(苄腈)络合物, 苯甲腈钯络合物

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About This Item

线性分子式:
(C6H5CN)2PdCl2
CAS号:
14220-64-5
分子量:
383.57
Beilstein:
3981730
EC 号:
238-085-3
MDL编号:
MFCD00013123
UNSPSC代码:
12161600
PubChem化学物质编号:
24853396
NACRES:
NA.22

质量水平

100

方案

95%

表单

powder

反应适用性

core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst

环保替代产品特性

Catalysis
Learn more about the Principles of Green Chemistry.

sustainability

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mp

131 °C (lit.)

环保替代产品分类

Aligned,

SMILES字符串

Cl[Pd]Cl.N#Cc1ccccc1.N#Cc2ccccc2

InChI

1S/2C7H5N.2ClH.Pd/c2*8-6-7-4-2-1-3-5-7;;;/h2*1-5H;2*1H;/q;;;;+2/p-2

InChI key

WXNOJTUTEXAZLD-UHFFFAOYSA-L

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相关类别

一般描述

二（苯腈）氯化钯（II）是一咱种配位化合物，在Suzuki交叉偶联反应中用作催化剂。


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应用

双（笨腈）氯化钯（II）可作为催化剂，用于：
  • 通过 Wacker 氧化，从末端烯烃更绿色环保地合成胺，然后转移氢化所得亚胺。
  • 交叉偶联反应 和 α-O-糖苷化。

末端烯烃的正式反马氏氢胺化反应

储存分类代码

11 - Combustible Solids

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable

个人防护装备

Eyeshields, Gloves, type N95 (US)

历史批次信息供参考:

分析证书(COA)

Lot/Batch Number
MKCW0545
0000315504
0000315504
MKCV6486
0000222742

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Catalysts of Suzuki Cross-Coupling Based on Functionalized Hyper-cross-linked Polystyrene: Influence of Precursor Nature
Nemygina N, et al.
Organic Process Research & Development, 20(8), 1453-1460 (2019)
Wei Shi et al.
Chemical communications (Cambridge, England), (23), 2342-2344 (2007-09-12)
A direct alkynylation of readily available alpha-halo esters and amides with high yields is described herein; a distinct switch from diyne formation to alkynylation products was attained under neutral conditions.
Brandon P Schuff et al.
Organic letters, 9(16), 3173-3176 (2007-07-10)
A novel method for palladium-catalyzed stereoselective formation of alpha-O-glycosides has been developed. This strategy relies on the palladium-biaryl phosphine catalyst-glycal donor complexation to control the anomeric selectivity. It does not depend on the nature of the protecting groups on the
Shih-Chieh Yeh et al.
Polymers, 11(12) (2019-12-11)
A crucial polymer intermediate, 4-[1-(4-hydroxyphenyl)cyclopentyl]-phenol (bisphenol CP), was developed from dicyclopentadiene (DCPD), a key byproduct of the C5 fraction in petrochemicals. On the basis of bisphenol CP, a diamine, 4,4'-((cyclopentane-1,1-diylbis(4,1-phenylene))bis(oxy))-dianiline (cyclopentyl diamine; CPDA) was subsequently obtained through a nucleophilic substitution
Synthesis, 803-803 (1992)

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