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223689

Sigma-Aldrich

二(氰基苯)二氯化钯(II)

greener alternative

95%

别名:

二(氰基苯)二氯化钯(II), 二氯化钯双（苯甲腈）, 二氯双（苯甲腈）钯, 二氯双（苯甲腈）钯 (II), 二苯甲腈二氯化钯, 双（苯甲腈）二氯化钯 (II), 双（苯腈）二氯化钯, 氯化钯(II)双(苄腈)络合物, 苯甲腈钯络合物

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About This Item

线性分子式:
(C6H5CN)2PdCl2
CAS号:
14220-64-5
分子量:
383.57
Beilstein:
3981730
EC 号:
238-085-3
MDL编号:
MFCD00013123
UNSPSC代码:
12161600
PubChem化学物质编号:
24853396
NACRES:
NA.22

质量水平

100

方案

95%

表单

powder

反应适用性

core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst

环保替代产品特性

Catalysis
Learn more about the Principles of Green Chemistry.

sustainability

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mp

131 °C (lit.)

环保替代产品分类

Aligned,

SMILES字符串

Cl[Pd]Cl.N#Cc1ccccc1.N#Cc2ccccc2

InChI

1S/2C7H5N.2ClH.Pd/c2*8-6-7-4-2-1-3-5-7;;;/h2*1-5H;2*1H;/q;;;;+2/p-2

InChI key

WXNOJTUTEXAZLD-UHFFFAOYSA-L

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相关类别

一般描述

二（苯腈）氯化钯（II）是一咱种配位化合物，在Suzuki交叉偶联反应中用作催化剂。


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应用

双（笨腈）氯化钯（II）可作为催化剂，用于：
  • 通过 Wacker 氧化，从末端烯烃更绿色环保地合成胺，然后转移氢化所得亚胺。
  • 交叉偶联反应 和 α-O-糖苷化。

末端烯烃的正式反马氏氢胺化反应

储存分类代码

11 - Combustible Solids

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable

个人防护装备

Eyeshields, Gloves, type N95 (US)

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分析证书(COA)

Lot/Batch Number
MKCW0545
0000315504
0000315504
MKCV6486
0000222742

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Brandon P Schuff et al.
Organic letters, 9(16), 3173-3176 (2007-07-10)
A novel method for palladium-catalyzed stereoselective formation of alpha-O-glycosides has been developed. This strategy relies on the palladium-biaryl phosphine catalyst-glycal donor complexation to control the anomeric selectivity. It does not depend on the nature of the protecting groups on the
Wei Shi et al.
Chemical communications (Cambridge, England), (23), 2342-2344 (2007-09-12)
A direct alkynylation of readily available alpha-halo esters and amides with high yields is described herein; a distinct switch from diyne formation to alkynylation products was attained under neutral conditions.
Catalysts of Suzuki Cross-Coupling Based on Functionalized Hyper-cross-linked Polystyrene: Influence of Precursor Nature
Nemygina N, et al.
Organic Process Research & Development, 20(8), 1453-1460 (2019)
Shih-Chieh Yeh et al.
Polymers, 11(12) (2019-12-11)
A crucial polymer intermediate, 4-[1-(4-hydroxyphenyl)cyclopentyl]-phenol (bisphenol CP), was developed from dicyclopentadiene (DCPD), a key byproduct of the C5 fraction in petrochemicals. On the basis of bisphenol CP, a diamine, 4,4'-((cyclopentane-1,1-diylbis(4,1-phenylene))bis(oxy))-dianiline (cyclopentyl diamine; CPDA) was subsequently obtained through a nucleophilic substitution
Synthesis, 803-803 (1992)

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