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HPLC: suitable
试验参数
sample preparation: Dispersive (QuEChERS)
sample/matrix: 10 g of pureed oranges (homogenized with rind); spike at 50 ppb (add 16.75 μL of a custom made pesticide mix, each analyte at 30 μg/mL)
extraction tube: Supel™ QuE Citrate (EN) Tube (55227-U)
extraction process: add 10 mL acetonitrile; shake for 1 minute; add contents of a Supel QuE citrate extraction tube (55227-U); shake immediately for 1 minute; centrifuge at 3200 rpm for 5 minutes
clean-up tube: Supel-Q™ PSA/C18 (55284-U)
clean-up process: transfer 0.7 mL of the acetonitrile layer into a Supel QuE Z-Sep/C18 cleanup tube (55284-U); shake for 1 minute; centrifuge at 5000 rpm for 5 minutes; (transfer 0.2 mL of the supernatant into an empty 1.5 mL centrifuge tube; add 0.2 mL of water; centrifuge at 5000 rpm for 2 minutes.)
column: Ascentis Express C18, 5 cm x 2.1 mm I.D., 2.7 μm particles (53822-U)
mobile phase: [A] 10 mM ammonium acetate in water; [B] 10 mM ammonium acetate in acetonitrile
gradient: Hold at 30% B for 1 min; 30% to 80% B in 2 min; hold at 80% B for 4 min; hold at 100% B for 3 min; hold at 30% B for 3 min
flow rate: 0.3 mL/min
pressure: 2730 psi (188 bar)
column temp.: 30 °C
detector: MS/MS, ESI positive
适用性
application for HPLC
应用
food and beverages
分析说明
法律信息
分析物
SPE 管或板
分析色谱柱
标准
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