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Merck
CN

55227-U

Supelco

Supel QuE QuEChERS tube

Citrate Extraction Tube, pk of 50, suitable for EN 15662

别名:

QuEChERS

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About This Item

UNSPSC代码:
41115712
NACRES:
NB.21

产品名称

Supel QuE, Citrate Extraction Tube, pk of 50, suitable for EN 15662

物料

polypropylene tube

质量水平

Agency

suitable for EN 15662

产品线

Supel

组成

magnesium sulfate, 4 g
sodium chloride, 1 g (Cat. No. S7653)
sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635)
sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)

包装

pk of 50

技术

QuEChERS: suitable

离心管体积

15 mL

应用

food and beverages

分离技术

ion exchange

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一般描述

分散SPE法,通常也是指"QuEChERS” 方法(快速,简便,便宜,有效,耐用和安全),是一种现代样本准备技术,正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。

使用QuEChERS方法,食品/农产品样本首先在水溶性溶剂(比如乙腈),在高盐(比如氯化钠和硫酸镁)和或者缓冲试剂(比如柠檬酸盐)存在下,进行提取。高盐能够引起液相分离,而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后,有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同,在分散SPE中,清洁需要混合大量的SPE(比如Supelclean PSA, ENVI-Carb, 和或者Discovery DSC-18)和提取物。 在样本清洁后,混合物经过离心,得到的上清可以直接分析,或者在分析前需要很少的处理。

Supelco有一系列的管和离心管,含有预置量的盐和SPE吸附剂,能够支持现今最常用的方法。

应用

Supel QuE柠檬酸盐小柱用于通过各种分析技术测定蔬菜上的农残。

适用性

适用于提取约10 g食品/农业样品。 柠檬酸盐用于缓冲萃取至pH 5.0-5.5。 在该pH下,大多数酸碱不稳定农药可保持稳定。

法律信息

Supel is a trademark of Sigma-Aldrich Co. LLC

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储存分类代码

13 - Non Combustible Solids

WGK

WGK 1

闪点(°F)

Not applicable

闪点(°C)

Not applicable


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分析证书(COA)

Lot/Batch Number

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Monitoring survey of the use patterns and pesticide residues on vegetables in the Niayes zone, Senegal
Diop A, et al.
Chemosphere, 144, 1715-1721 (2016)
Pesticide analysis at ppt concentration levels: coupling nano-liquid chromatography with dielectric barrier discharge ionization-mass spectrometry
Mirabelli.FM, et al.
Analytical and Bioanalytical Chemistry, 408(13), 3425-3434 (2016)
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
M Picot Groz et al.
The Science of the total environment, 493, 162-169 (2014-06-20)
The UV filters and musk fragrances have come into focus because these compounds are contained and increasingly used not only in sunscreen products but also in many products of daily use, such as cosmetics, skin creams, plastics or varnish. In

商品

Rapid & accurate analysis of 208 pesticides and their metabolites in a fruit sample using Supel™ QuE QuEChERS mixes for sample preparation and GC-MS/MS.

Pesticide residue analysis of 331 pesticides and 44 metabolites in cabbage samples using Supel™ QuE QuEChERS mixes and Purospher® STAR RP-18e column.

Pistachios 45% fat complicates pesticide analysis. But Z-Sep+ sorbent cleanup after QuEChERS extraction can reduce background for reliable results.

Dual-layer cartridge achieves efficient SPE clean-up for challenging pesticide residue testing in turmeric and spices.

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相关内容

QuEChERS is a ‘Quick, Easy, Cheap, Effective, Rugged and Safe’ sample cleanup method used to prepare food and agricultural samples for pesticides analysis. QuEChERS is based on the Solid Phase Extraction (SPE) technique of sample preparation.

QuEChERS方法简化了食品和农业样品农残分析的样品纯化步骤。

Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.

固相萃取(SPE)是一种用在色谱分析(如 HPLC、GC、TLC 色谱)前快速、选择性制备和纯化样品的技术,主要用于置换样品基质、浓缩分析物、去除干扰成分和污染物,以改善数据结果、保护分析色谱柱。

Chromatograms

application for HPLCapplication for HPLC, application for SPE

我们的科学家团队拥有各种研究领域经验,包括生命科学、材料科学、化学合成、色谱、分析及许多其他领域.

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