GC Analysis of Fluoxetine Enantiomers (N-TFA Derivatives) on Astec^® CHIRALDEX^™ B-DA

column

Astec CHIRALDEX B-DA, 10 m x 0.25 mm I.D., 0.12 μm (72021AST)

oven

175 °C

detector

FID, 250 °C

carrier gas

helium, 15 psi

inj. temp.

250 °C

sample

peaks 1 & 2: fluoxetine enantiomers (N-TFA derivatives)