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Merck
CN

25351

Supelco

SPB®-5毛细管GC色谱柱

L × I.D. 60 m × 0.53 mm, df 5.00 μm

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About This Item

UNSPSC代码:
41115710
eCl@ss:
32119290

物料

fused silica

质量水平

Agency

meets requirements for USP G27 and G36

参数

-60-260 °C temperature (isothermal)
-60-280 °C temperature (programmed)

β值

27

df

5.00 μm

技术

gas chromatography (GC): suitable

长度 × 内径

60 m × 0.53 mm

基质活性基团

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

色谱柱类型

capillary non-polar

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一般描述

应用:这种非极性通用色谱柱主要使得组份按照沸点高低顺序洗脱,选择性略有提高,特别适用于芳香族化合物。
USP 代码:本色谱柱符合 USP G27 和 G36 要求。

  • 结合的
  • 聚(5% 二苯基/ 95% 二甲基硅氧烷)
温度限制
  • ≤0.32mm 内径,<2 μm:-60°C 至 320°C(等温或程序化)
  • ≤0.32mm 内径,<2 μm:-60°C 至 300°C(等温或程序化)
  • ≥0.53mm 内径,<2 μm:-60°C 至 300°C(等温)或 320°C(程序化)
  • ≥0.53mm 内径,<2 μm:-60°C 至 260°C(等温)或 280°C(程序化)
Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.

应用

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

其他说明

We offer a variety of chromatography accessories including analytical syringes

法律信息

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

储存分类代码

11 - Combustible Solids

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable


历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography
SCott PM
Journal - Association of Official Analytical Chemists, 889-893 (1985)
Á Kenéz et al.
Journal of dairy science, 102(12), 11718-11729 (2019-09-30)
Adipose tissue response to endocrine stimuli, such as insulin, is crucial for metabolic adaptation at the onset of lactation in dairy cows. However, the exact molecular mechanisms behind this response are not well understood. Thus, the aim of this study
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
Zhihua Fan et al.
Environmental science & technology, 40(19), 6051-6057 (2006-10-21)
A sensitive, simple, and cost-effective passive sampling methodology was developed to quantify personal exposure to gaseous polycyclic aromatic hydrocarbons (PAHs). A Fan-Lioy passive PAH sampler (FL-PPS) is constructed from 320 sections of 1-cm long SPB-5 GC columns (0.75-mm i.d. and
V Gajdůsková et al.
Veterinarni medicina, 37(8), 471-478 (1992-08-01)
Occurrence of individual polychlorinated biphenyl (PCB) congeners in the environment, foodstuffs and other biological materials was assessed. Analysis of specific PCB congeners (28, 52, 101, 138, 153, 180), occurring in animal raw materials and foodstuffs most frequently, has been implemented.

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