material
fused silica
agency
meets requirements for USP G27 and G36
parameter
-60-320 °C temperature (isothermal or programmed)
Beta value
250
df
0.20 μm
technique(s)
gas chromatography (GC): suitable
L × I.D.
30 m × 0.20 mm
matrix active group
Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase
column type
capillary non-polar
Quality Level
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General description
应用：这种非极性通用色谱柱主要使得组份按照沸点高低顺序洗脱，选择性略有提高，特别适用于芳香族化合物。
USP 代码：本色谱柱符合 USP G27 和 G36 要求。
相：
USP 代码：本色谱柱符合 USP G27 和 G36 要求。
相：
- 结合的
- 聚（5％ 二苯基/ 95％ 二甲基硅氧烷）
- ≤0.32mm 内径，<2 μm：-60°C 至 320°C（等温或程序化）
- ≤0.32mm 内径，<2 μm：-60°C 至 300°C（等温或程序化）
- ≥0.53mm 内径，<2 μm：-60°C 至 300°C（等温）或 320°C（程序化）
- ≥0.53mm 内径，<2 μm：-60°C 至 260°C（等温）或 280°C（程序化）
Application
SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.
Other Notes
We offer a variety of chromatography accessories including analytical syringes
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
V Gajdůsková et al.
Veterinarni medicina, 37(8), 471-478 (1992-08-01)
Occurrence of individual polychlorinated biphenyl (PCB) congeners in the environment, foodstuffs and other biological materials was assessed. Analysis of specific PCB congeners (28, 52, 101, 138, 153, 180), occurring in animal raw materials and foodstuffs most frequently, has been implemented.
D Marrero Delange et al.
Journal of chromatography. B, Biomedical sciences and applications, 762(1), 43-49 (2001-10-09)
1-Octacosanol is the major component of policosanol, a new natural lowering-cholesterol agent. A sensitive solid-phase extraction with a Tenax GC capillary gas chromatography method for determining the proportion of this fatty alcohol in plasma after its denaturation with trichloroacetic acid
P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
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