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质量水平
反应适用性
reaction type: Grignard Reaction
浓度
1.0 M in THF
bp
65-67 °C
密度
0.998 g/mL at 25 °C
SMILES字符串
Cc1cccc(C)c1[Mg]Br
InChI
1S/C8H9.BrH.Mg/c1-7-4-3-5-8(2)6-7;;/h3-5H,1-2H3;1H;/q;;+1/p-1
InChI key
BIGUVDUZGAJWQK-UHFFFAOYSA-M
应用
2,6-Dimethylphenylmagnesium bromide can be used:
- As an intermediate in the synthesis of dibutyl(5,10-dihydro-1,9-di-p-toluoyl-5-p-tolyldipyrrinato)tin(IV), which is further used in the preparation of zinc-based porphyrin.
- As a substrate in the preparation of substituted fluorenes by reacting with 2-substituted arenesulfonates and dihaloarenes.
警示用语：
Danger
危险分类
Acute Tox. 3 Inhalation - Acute Tox. 4 Oral - Carc. 2 - Flam. Liq. 2 - Skin Corr. 1B - STOT SE 3 - Water-react 2
靶器官
Respiratory system
补充剂危害
WGK
WGK 3
闪点(°F)
-2.2 °F
闪点(°C)
-19 °C
个人防护装备
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
法规信息
危险化学品
Pd (OAc) 2-catalyzed domino reactions of 1, 2-dihaloarenes and 2-haloaryl arenesulfonates with Grignard reagents: efficient synthesis of substituted fluorenes
Dong C and Hu Q
Tetrahedron, 64(11), 2537-2552 (2008)
Nearly Chromatography-Free Synthesis of the A3B-Porphyrin 5-(4-Hydroxymethylphenyl)-10, 15, 20-tri-p-tolylporphinatozinc (II).
Zaidi SHH, et al.
Organic Process Research & Development, 10(2), 304-314 (2006)
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