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等级
for GC derivatization
synthesis grade
质量水平
蒸汽密度
>1 (vs air)
蒸汽压
8.8 mmHg ( 27 °C)
检测方案
≥98%
形式
liquid
反应适用性
reagent type: derivatization reagent
reaction type: Silylations
折射率
n20/D 1.38 (lit.)
bp
130-132 °C (lit.)
密度
1.075 g/mL at 25 °C (lit.)
储存温度
2-8°C
SMILES字符串
CN(C(=O)C(F)(F)F)[Si](C)(C)C
InChI
1S/C6H12F3NOSi/c1-10(12(2,3)4)5(11)6(7,8)9/h1-4H3
InChI key
MSPCIZMDDUQPGJ-UHFFFAOYSA-N
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一般描述
N-甲基-N-(三甲基硅烷基)三氟乙酰胺(MSTFA)是一种衍生化试剂。它可以用作重氮甲烷的替代品。
应用
甲硅烷基化试剂可用于生成GC-MS分析用挥发性衍生物。
用于同时检测类固醇激素17-α-乙炔雌二醇和雌酮的改良型甲硅烷基化程序。
用于同时检测类固醇激素17-α-乙炔雌二醇和雌酮的改良型甲硅烷基化程序。
其他说明
三甲基甲硅烷基化试剂。
警示用语:
Warning
危险分类
Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
WGK
WGK 3
闪点(°F)
78.8 °F
闪点(°C)
26 °C
个人防护装备
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
危险化学品
Environment international, 31(5), 679-685 (2005-05-25)
Pharmacologically active substances used to treat human and animal illnesses can enter the aquatic environment via effluents from wastewater treatment plants or in the case of veterinary drugs directly through liquid manure discharge. Some of these substances enter the environment
Journal of chromatography. A, 1247, 118-124 (2012-06-15)
GC-MS analysis of silylated metabolites is a sensitive method that covers important metabolite groups such as sugars, amino acids and non-amino organic acids, and it has become one of the most important analytical methods for exploring the metabolome. Absolute quantitative
Journal of chromatography. A, 1217(11), 1748-1760 (2010-02-13)
An alternative method for the sensitive determination of several drugs of abuse and some of their metabolites in surface and sewage water samples is proposed. Analytes are concentrated using a solid-phase extraction (SPE) sorbent, converted into the corresponding trimethylsilyl derivatives
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 871(2), 191-201 (2008-06-10)
Metabolomics being the most recently introduced "omic" analytical platform is currently at its development phase. For the metabolomics to be broadly deployed to biological and clinical research and practice, issues regarding data validation and reproducibility need to be resolved. Gas
Journal of chromatography. A, 1131(1-2), 192-202 (2006-08-08)
A novel method has been developed to simultaneously determine and quantify seven organic UV filters employing liquid (solid)-liquid extraction, derivatization with N-methyl-N-(trimethylsilyl) trifluoroacetamide (MSTFA) and gas chromatography with mass spectrometric detection in various environmental matrices. The UV filters determined were:
实验方案
Alkylphenols are used in various industries like paper manufacturing and pesticide formulations.
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