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Key Documents

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178721

Sigma-Aldrich

(Diacetoxyiodo)benzene

98%

Synonym(s):

Iodobenzene I,I-diacetate, Iodosobenzene I,I-diacetate

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100 MG
¥785.64

¥785.64

Available to ship on2025年4月24日Details

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100 MG
¥785.64

About This Item

Linear Formula:
C6H5I(O2CCH3)2
CAS Number:
3240-34-4
Molecular Weight:
322.10
Beilstein:
1879369
EC Number:
221-808-1
MDL number:
MFCD00008692
UNSPSC Code:
12352002
PubChem Substance ID:
24850764
NACRES:
NA.22

¥785.64

Available to ship on2025年4月24日Details

Request a Bulk Order

Quality Level

200

Assay

98%

form

powder

reaction suitability

reagent type: catalyst
reagent type: oxidant
reaction type: C-H Activation

mp

161-163 °C (lit.)

functional group

iodo

SMILES string

CC(OI(OC(C)=O)C1=CC=CC=C1)=O

InChI

1S/C10H11IO4/c1-8(12)14-11(15-9(2)13)10-6-4-3-5-7-10/h3-7H,1-2H3

InChI key

ZBIKORITPGTTGI-UHFFFAOYSA-N

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344827

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喹吖因 二盐酸盐 A non-specific phospholipase A2 (PLA2) inhibitor.

551850

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Diltiazem, Hydrochloride Synthetic benzothiazepine that acts as an L-type Ca2+ channel antagonist.

309866

Diltiazem, Hydrochloride

assay

≥99%

assay

≥98% (NMR)

assay

≥98% (HPLC)

assay

≥98% (HPLC)

manufacturer/tradename

Calbiochem®

manufacturer/tradename

Calbiochem®

manufacturer/tradename

Calbiochem®

manufacturer/tradename

Calbiochem®

Quality Level

100

Quality Level

300

Quality Level

100

Quality Level

100

storage temp.

10-30°C

storage temp.

−20°C

storage temp.

10-30°C

storage temp.

10-30°C

storage condition

OK to freeze, protect from light

storage condition

OK to freeze, protect from light

storage condition

OK to freeze, desiccated (hygroscopic), protect from light

storage condition

OK to freeze, desiccated (hygroscopic)

Application

Rh2(esp)2: An Exceptionally Efficient and Selective Catalyst for C-H Amination
Stoichiometric oxidant in the TEMPO oxidation of nerol to neral.[1] Oxidant employed in the rhodium-catalyzed aziridination of olefins with sulfamate esters.[2]
Unactivated sp3 C-H bonds of both oxime and pyridine substrates undergo highly regio- and chemoselective Pd(II)-catalyzed oxygenation with PhI(OAc)2 as a stoichiometric oxidant.[3]
Used in the room temperature Pd-catalyzed 2-arylation of indoles
Useful reagent for the synthesis of a wide variety of heterocyclic compounds.[4][5]

related product

Product No.
Description
Pricing

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves
  • Specification Sheet

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    Certificates of Analysis (COA)

    Lot/Batch Number
    0000427490
    0000427501
    0000427490
    0000427501
    0000379493

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    Determination of vitamin C in tablets and fruits by titration with phenyliodosoacetate.
    S K Vaidya et al.
    Il Farmaco; edizione pratica, 37(1), 9-14 (1982-01-01)
    Hai Yi et al.
    Chemical communications (Cambridge, England), 46(37), 6941-6943 (2010-08-24)
    3-Aryl-4-unsubstituted-6-CF(3)-pyridin-2-ones have been efficiently synthesized from readily available 4-aryl-3-carbamoyl-6-CF(3)-pyridin-2(1H)-ones by treatment with PhI(OAc)(2) in the presence of NaOH.
    Aldrichimica Acta, 27, 15-15 (1994)
    Chunying Gao et al.
    Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 1060, 158-165 (2017-06-18)
    25-hydroxyvitamin D3-3-sulfate (25-OHD3-S) and 25-hydroxyvitamin D3-3-glucuronide (25-OHD3-G) are major conjugative metabolites of vitamin D3 found in the systemic circulation and potentially important reservoirs for 25-hydroxyvitamin D3. Simultaneous and accurate quantification of these metabolites could advance assessment of the impact of
    Lopa V Desai et al.
    Journal of the American Chemical Society, 126(31), 9542-9543 (2004-08-05)
    This communication describes a new palladium-catalyzed method for the oxygenation of unactivated sp3 C-H bonds. A wide variety of alkane substrates containing readily available oxime and/or pyridine directing groups are oxidized with extremely high levels of chemo-, regio-, and in
    View All Related Papers

    Articles

    Rh2(esp)2 Catalyst

    New! Rh2(esp)2, and exceptionally efficient and selective catalyst for C-H amination.

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