GC Analysis of PCB Congeners in Stream Sediment on SPB®-Octyl after SPME using 100 μm PDMS Fiber
CONDITIONS
sample/matrix
5 g stream sediment, downstream from industrial sites
SPME fiber
PDMS, 100 μm (57300-U) (57300-U)
extraction
headspace, 90 °C/30 min
desorption process
280 °C/2 min, splitless
column
SPB®-Octyl, 30 m × 0.25 mm I.D., 0.25 μm (24218-U)
oven
50 °C/1 min at 10 °C/min to 150 °C/0 min
说明
法律信息
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany