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Merck
CN

G005912

LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Set 3

application for HPLC

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About This Item

技术

HPLC: suitable

试验参数

column: Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)
mobile phase: [A] 5 mM ammonium formate in acetonitrile; [B] water; (98:2, A:B)
flow rate: 0.6 mL/min
pressure: 267 psi (18.4 bar)
column temp.: 35 °C
detector: MS, ESI(+) TOF, Summed Ion Chromatogram
injection: 2 μL
sample: 500 ng/mL in acetonitrile

适用性

application for HPLC

应用

forensics and toxicology

分析说明

HILIC mode operation on an Ascentis Express column provided baseline resolution of these bath salts, including isobaric compounds. The highest quality LC-MS solvents were used to supply low background interference and low particulate contaminants for robust; trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.

法律信息

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

分析物

说明

    Pentedrone hydrochloride, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
    3-Fluoromethcathinone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
    4-Methylethcathinone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
    4-Fluoromethcathinone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
    3,4-Dimethylmethcathinone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

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