推荐产品
product name
Supel™ QuE, Z-Sep+ Tube, pk of 50, centrifuge tube volume 15 mL , Shaker Compatible
物料
polypropylene tube
质量水平
产品线
Supel™
组成
Z-Sep+, 500 mg
包装
pk of 50
技术
QuEChERS: suitable
离心管体积
15 mL , Shaker Compatible
基质活性基团
zirconia-based phase
应用
food and beverages
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一般描述
分散SPE法，通常也是指"QuEChERS” 方法（快速，简便，便宜，有效，耐用和安全），是一种现代样本准备技术，正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。
使用QuEChERS方法，食品/农产品样本首先在水溶性溶剂（比如乙腈），在高盐（比如氯化钠和硫酸镁）和或者缓冲试剂（比如柠檬酸盐）存在下，进行提取。高盐能够引起液相分离，而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后，有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同，在分散SPE中，清洁需要混合大量的SPE（比如Supelclean PSA, ENVI-Carb， 和或者Discovery DSC-18）和提取物。 在样本清洁后，混合物经过离心，得到的上清可以直接分析，或者在分析前需要很少的处理。
Supelco有一系列的管和离心管，含有预置量的盐和SPE吸附剂，能够支持现今最常用的方法。
使用QuEChERS方法，食品/农产品样本首先在水溶性溶剂（比如乙腈），在高盐（比如氯化钠和硫酸镁）和或者缓冲试剂（比如柠檬酸盐）存在下，进行提取。高盐能够引起液相分离，而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后，有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同，在分散SPE中，清洁需要混合大量的SPE（比如Supelclean PSA, ENVI-Carb， 和或者Discovery DSC-18）和提取物。 在样本清洁后，混合物经过离心，得到的上清可以直接分析，或者在分析前需要很少的处理。
Supelco有一系列的管和离心管，含有预置量的盐和SPE吸附剂，能够支持现今最常用的方法。
相容性
Compatible with most QuEChERS shakers.
其他说明
Supel™ QuE Z-Sep products enhance sample cleanup for complex matrices by effectively removing more fat and color from sample extracts than traditional phases for QuEChERS methods. By eliminating problematic matrix interferences, Z-Sep products provide more robust LC-MS and GC-MS methods. This proprietary technology can replace C18 and PSA in your current methods without additional method development.
Z-Sep+ is recommended for cleanup of samples containing greater than 15% fat.
Z-Sep/C18 is recommended for cleanup of samples containing less than 15% fat.
Z-Sep is recommended for cleanup of samples prior to analysis of hydrophobic analytes.
Z-Sep+ is recommended for cleanup of samples containing greater than 15% fat.
Z-Sep/C18 is recommended for cleanup of samples containing less than 15% fat.
Z-Sep is recommended for cleanup of samples prior to analysis of hydrophobic analytes.
法律信息
Certain uses of this product may be covered by the claims of one or more pending patent applications. For licensing inquiries please contact techserv@sial.com
AOAC is a registered trademark of AOAC International
Supel is a trademark of Sigma-Aldrich Co. LLC
WGK
nwg
闪点(°F)
Not applicable
闪点(°C)
Not applicable
Martina Rejtharová et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 35(2), 233-240 (2017-10-06)
A sensitive and robust confirmatory method for determination of steroid esters in blood serum is essential for reliable monitoring of possible illegal use of steroid hormones as growth promoters in meat production. A previously used sample preparation methodology was improved.
Ana Lozano et al.
Talanta, 118, 68-83 (2013-11-28)
Two sorbents containing ZrO₂ (Z-Sep and Z-Sep+) were tested as a d-SPE clean-up in combination with the QuEChERS and ethyl acetate multiresidue method in the pesticide residues extraction in avocado. All extracts were analysed using gas chromatography coupled with a
Piotr Kaczynski et al.
Ecotoxicology and environmental safety, 139, 124-131 (2017-01-28)
Highly toxic insecticides (HTIs) belonging to different chemical groups are dangerous to pollinating organisms, even in sublethal doses. An important objective of this study was to develop a method to determine over fifty HTIs at very low concentrations in the
Yin-E Liu et al.
Journal of chromatography. A, 1532, 68-73 (2017-12-13)
An analytical method has been developed for measuring 12 organophosphorus flame retardants (PFRs) in fish tissue samples. After the Soxhlet extraction of PFRs with dichloromethane. The experimental parameters of the clean-up were systematically optimized. Methanol was found to be a
Pol Herrero et al.
Journal of chromatography. A, 1339, 34-41 (2014-03-25)
A Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction method followed by liquid chromatography-(Orbitrap) high resolution mass spectrometry was developed for the simultaneous determination of five benzotriazole, four benzothiazole and five benzenesulfonamide derivates in sewage sludge. While the method
商品
Pistachios 45% fat complicates pesticide analysis. But Z-Sep+ sorbent cleanup after QuEChERS extraction can reduce background for reliable results.
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