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55299-U

Supelco

Supel QuE QuEChERS tube

Z-Sep+ Bulk, pkg of 20 g

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别名:
QuEChERS
EC 号:
UNSPSC代码:
41115712
NACRES:
NB.21

product name

Supel QuE, Z-Sep+ Bulk, pkg of 20 g

物料

polypropylene tube

质量水平

产品线

Supel

组成

Z-Sep+ Bulk

包装

pkg of 20 g

技术

QuEChERS: suitable

表面积

480 m2/g

基质

silica gel base material

基质活性基团

zirconia-based phase

粒径

50 μm

孔径

70 Å pore size

应用

food and beverages

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一般描述

分散SPE法,通常也是指"QuEChERS” 方法(快速,简便,便宜,有效,耐用和安全),是一种现代样本准备技术,正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。

使用QuEChERS方法,食品/农产品样本首先在水溶性溶剂(比如乙腈),在高盐(比如氯化钠和硫酸镁)和或者缓冲试剂(比如柠檬酸盐)存在下,进行提取。高盐能够引起液相分离,而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后,有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同,在分散SPE中,清洁需要混合大量的SPE(比如Supelclean PSA, ENVI-Carb, 和或者Discovery DSC-18)和提取物。 在样本清洁后,混合物经过离心,得到的上清可以直接分析,或者在分析前需要很少的处理。

Supelco有一系列的管和离心管,含有预置量的盐和SPE吸附剂,能够支持现今最常用的方法。

其他说明

与 QuEChERS LC-MS 方法的传统相相比,Supel QuE Z-Sep + 可有效去除样本萃取物中更多的脂肪和颜色,从而提高样本对复杂基质的清除能力。通过消除有问题的基质干扰,Z-Sep 产品提供了更稳健的 LC-MS 方法。这种专有技术可以替代当前方法中的C18和PSA,无需额外的方法开发。

建议使用 Z-Sep + 清除脂肪含量超过 15% 的样本。

法律信息

本产品的某些用途可能包含在一项或多项未决专利申请的权利要求中。如需许可咨询,请联系techserv@sial.com
Supel is a trademark of Sigma-Aldrich Co. LLC

WGK

nwg

闪点(°F)

Not applicable

闪点(°C)

Not applicable

法规信息

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Pol Herrero et al.
Journal of chromatography. A, 1339, 34-41 (2014-03-25)
A Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction method followed by liquid chromatography-(Orbitrap) high resolution mass spectrometry was developed for the simultaneous determination of five benzotriazole, four benzothiazole and five benzenesulfonamide derivates in sewage sludge. While the method
Łukasz Rajski et al.
Journal of chromatography. A, 1304, 109-120 (2013-07-23)
Several extraction methods were evaluated in terms of recoveries and extraction precision for 113 pesticides in avocado: QuEChERS with various d-SPE clean-ups (Z-Sep, Z-Sep+, PSA+C18 and silica), miniLuke and ethyl acetate. Extracts were analysed using liquid chromatography coupled with triple
Keiko Iwakoshi et al.
Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan, 57(5), 150-154 (2016-10-28)
Rapid multi-residue analysis of pesticides in pulses was developed using LC-MS/MS. Pesticide residues in 5 g of homogenized pulses were extracted with 30 mL of acetonitrile and salted out with 4 g of anhydrous magnesium sulfate and 2 g of
José Fernando Huertas-Pérez et al.
Journal of pharmaceutical and biomedical analysis, 124, 261-266 (2016-03-13)
A simple, effective and reliable method for the determination of eight sulfonamide antibiotics (sulfadiazine, sulfapiridine, sulfamerazine, sulfamethazine, sulfachloropiridazine, sulfamethoxazole, sulfadoxine, sulfadimethoxin) in chicken muscle and eggs by liquid chromatography and fluorescence detection has been developed and validated. Sulfonamides do not
Martina Rejtharová et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 35(2), 233-240 (2017-10-06)
A sensitive and robust confirmatory method for determination of steroid esters in blood serum is essential for reliable monitoring of possible illegal use of steroid hormones as growth promoters in meat production. A previously used sample preparation methodology was improved.

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