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Merck
CN

46401-U

消旋-β-生育酚 溶液

50 mg/mL in hexane, certified reference material

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化学文摘社编号:
148-03-8
MDL number:
MFCD00036171
UNSPSC Code:
85151701
eCl@ss:
34058016
NACRES:
NA.24

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产品名称

消旋-β-生育酚 溶液, 50 mg/mL in hexane, certified reference material

SMILES string

O1[C@@](CCc2c1c(cc(c2C)O)C)(CCCC(CCCC(CCCC(C)C)C)C)C

InChI

1S/C28H48O2/c1-20(2)11-8-12-21(3)13-9-14-22(4)15-10-17-28(7)18-16-25-24(6)26(29)19-23(5)27(25)30-28/h19-22,29H,8-18H2,1-7H3/t21?,22?,28-/m1/s1

InChI key

WGVKWNUPNGFDFJ-CBIUGAAKSA-N

grade

certified reference material

CofA

current certificate can be downloaded

packaging

ampule of 1 mL

concentration

50 mg/mL in hexane

technique(s)

HPLC: suitable
gas chromatography (GC): suitable

application(s)

pharmaceutical (small molecule)
vitamins, nutraceuticals, and natural products

format

single component solution

storage temp.

-10 to -25°C

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Application

该分析标准品溶液可用于以下应用：
  • 通过超高效液相色谱（UHPLC）和荧光检测在液液萃取（LLE）后同时测定人血清样品中的维生素A和所有四种生育酚异构体
  • 通过液相色谱电喷雾电离/多级质谱（LC-ESI-MS/MS）进行四种不同小麦品种中麦草和麦粒样品的维生素B（B1、B2、B5和B9）和维生素 E （α-生育酚、β-生育酚、α-三烯生育酚和β-三烯生育酚）的多残留分析
  • 通过非水反相高效液相色谱（NARP-HPLC）和大气压化学电离-串联质谱（APCI-MS/MS）检测分离和评估沟美洲山核桃栽培样品中的四种生育酚和四种三烯生育酚
  • 通过化学计量法辅助的优化高效液相色谱（HPLC）和荧光检测方法分析不同冷榨油样品以检测和定量测定八种母育酚同系物
  • 开发和确定正相高效液相色谱（NP-HPLC）方法，该方法和荧光检测一起使用可以同时测定芝麻油样品中的四种生育酚和四种木酚素。

General description

β-生育酚是脂溶形式的维生素E，具有抗氧化、抗炎、抗细胞增殖和抗癌特性。

signalword

Danger

Hazard Classifications

Aquatic Chronic 2 - Asp. Tox. 1 - Flam. Liq. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 1 Inhalation - STOT SE 3

target_organs

Central nervous system, Nervous system

存储类别

3 - Flammable liquids

wgk

WGK 3

flash_point_f

-9.4 °F - closed cup

flash_point_c

-23 °C - closed cup

ppe

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

法规信息

危险化学品
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Qualitative and quantitative analysis of retinol, retinyl esters, tocopherols and selected carotenoids out of various internal organs from different species by HPLC
Schaffer MW, et al.
Analytical Methods : Advancing Methods and Applications, 2(9), 1320-1332 (2010)
Analysis of the components of pumpkin seed oil in suppositories and the possibility of its use in pharmaceuticals
A.O.V, et al.
Journal of Chemical and Pharmaceutical Research , 6(5), 1106-1116 (2014)
Rapid determination of lipophilic vitamins in human serum by ultra-high performance liquid chromatography using a fluorinated column and high-throughput miniaturized liquid-liquid extraction
Cervinkova B, et al.
Journal of Separation Science, 40(17), 3375-3382 (2017)
Pressurized liquid extraction and dispersive liquid-liquid microextraction for determination of tocopherols and tocotrienols in plant foods by liquid chromatography with fluorescence and atmospheric pressure chemical ionization-mass spectrometry detection
Vi?as P, et al.
Talanta, 119(9), 98-104 (2014)
Xiaofeng Fang et al.
Developmental cell, 48(3), 371-382 (2019-01-01)
As integral regulators in plant development and stress response, microRNAs (miRNAs) themselves need to be tightly regulated. Here, we show that tocopherols (vitamin E), lipid-soluble antioxidants synthesized from tyrosine in chloroplasts, positively regulate the biogenesis of miRNAs. Tocopherols are required

实验方案

HPLC Determination of Vitamin A and E

GB method with Ascentis® Express C30 column achieves baseline resolution for Vitamin A and E critical pair.

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