等级
for GC derivatization
描述
Silyl reagent
包装
pkg of 400 mL
浓度
5% dimethyldichlorosilane in toluene
SMILES字符串
C[Si](C)(Cl)Cl
InChI
1S/C2H6Cl2Si/c1-5(2,3)4/h1-2H3
InChI key
LIKFHECYJZWXFJ-UHFFFAOYSA-N
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一般描述
For deactivating glassware.
Treat the glass tubing that you use for columns with Sylon-CT solution (5% dimethyldichlorosilane in toluene). It deactivates the tubing for use up to 350 °C to 400 °C, far exceeding the capabilities of other deactivating agents used at room temperature. Sylon CT™ also deactivates transfer lines and glass or glass-lined injection port liners. Instructions included.
Treat the glass tubing that you use for columns with Sylon-CT solution (5% dimethyldichlorosilane in toluene). It deactivates the tubing for use up to 350 °C to 400 °C, far exceeding the capabilities of other deactivating agents used at room temperature. Sylon CT™ also deactivates transfer lines and glass or glass-lined injection port liners. Instructions included.
应用
Sylon CT™ was used as derivatizing agent, during an experiment to develop sensitive GC method for the identification and determination of long-chain primary alkyl amines. It was also used for treating Erlenmeyer flasks to prevent mycelium from sticking to the glassware during development of techniques in the identification and partial characterization the chaxamycin biosynthesis gene cluster of S. leeuwenhoekii.
法律信息
Sylon CT is a trademark of Sigma-Aldrich Co. LLC
警示用语：
Danger
危险分类
Aquatic Chronic 3 - Asp. Tox. 1 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - Skin Corr. 1A - STOT RE 2 - STOT SE 3
靶器官
Central nervous system
补充剂危害
WGK
WGK 3
闪点(°F)
39.2 °F
闪点(°C)
4 °C
个人防护装备
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
法规信息
新产品
Peter Kusch et al.
Journal of chromatography. A, 1113(1-2), 198-205 (2006-02-18)
Gas chromatography with simultaneous flame-ionization detection (FID) and a nitrogen-phosphorus detection (NPD) as well as gas chromatography-mass spectrometry (GC/MS) has been used to characterize long-chain primary alkyl amines after derivatization with trifluoroacetic anhydride (TFAA). Electron impact ionization- (EI) and negative
Teemu Näykki
Analytical and bioanalytical chemistry, 372(7-8), 829-831 (2002-05-16)
The use of silylation of glassware in mercury analytics was investigated. By treating the glassware with 5% (v/v) dichlorodimethylsilane in toluene, the surfaces of the vessels were inactivated. Method development proved that silylation can extend the range of stabile, contamination-free
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