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Merck
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安全信息

33040-U

Supelco

三氟化硼-甲醇

10 % (w/w)

别名:

三氟化硼

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About This Item

UNSPSC代码:
12000000

等级

for GC derivatization

反应适用性

reagent type: derivatization reagent
reaction type: Alkylations

reagent type: derivatization reagent
reaction type: Esterifications

包装

pkg of 10 × 5 mL

浓度

10 % (w/w)

储存温度

2-8°C

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一般描述

Boron trifluoride is a colourless gas and it reacts readily with water to form hydrates. It has been widely used as a catalyst during polymerizations, alkylations and condensation reactions. It is used as gas flux for internal soldering or brazing. It also finds application in being used as extinguisher for magnesium fires.

应用

It was used in transmethylation of 1,2-Diacylglycerol (DAG) containing fractions which were purified using HPLC. It may be used to treat lipids during GC analysis done for determination of fatty acid methyl esters and dimethylacetals.

其他说明

Reagent for O-acetyl, methyl ester, methyl 2,2-dimethoxypropionate, dimethyl acetals and dimethoxy.

警示用语:

Danger

危险分类

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A - STOT RE 2 Inhalation - STOT SE 1

靶器官

Eyes, Kidney

WGK

WGK 2

闪点(°F)

closed cup

闪点(°C)

closed cup

个人防护装备

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

法规信息

危险化学品

Choose from one of the most recent versions:

分析证书(COA)

Lot/Batch Number

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在文件库中查找您最近购买产品的文档。

访问文档库

D.R. Knapp
Handbook of Analytical Derivatization Reactions, 438-438 (1979)
S B Bocckino et al.
The Journal of biological chemistry, 260(26), 14201-14207 (1985-11-15)
1,2-Diacylglycerol (DAG) was measured in neutral lipid extracts from isolated hepatocytes using high pressure liquid chromatography followed by refractive index detection. Maximally effective doses of epinephrine, angiotensin II, and vasopressin increased DAG by approximately 65, 80, and 180-250%, respectively, with
PREPARATION OF FATTY ACID METHYL ESTERS AND DIMETHYLACETALS FROM LIPIDS WITH BORON FLUORIDE--METHANOL.
W R MORRISON et al.
Journal of lipid research, 5, 600-608 (1964-10-01)
ANALYSIS OF HYDROXY FATTY ACIDS BY GAS-LIQUID CHROMATOGRAPHY.
J S O'BRIEN et al.
Analytical biochemistry, 7, 288-296 (1964-03-01)
Compressed Gas Association
Handbook of Compressed Gases, 271-271 (2012)

实验方案

鱼油胶囊和鲑鱼中ω-3脂肪酸的色谱分析,重点是通过使用两种不同选择性的GC色谱柱为分析师提供期望的验证性分析。

Analyze omega 3 fatty acid profiles from fish oil capsules and salmon using GC columns for confirmatory analysis of lipid composition.

Chromatograms

suitable for GCsuitable for GCsuitable for GC, application for SPEsuitable for GC展开

我们的科学家团队拥有各种研究领域经验,包括生命科学、材料科学、化学合成、色谱、分析及许多其他领域.

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