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Merck
CN

PHR1657

林可霉素 盐酸盐 一水合物

Pharmaceutical Secondary Standard; Certified Reference Material

别名:

Lincomycin hydrochloride monohydrate

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关于此项目

经验公式（希尔记法）:
C18H34N2O6S · HCl · H2O
化学文摘社编号:
7179-49-9
分子量:
461.01
NACRES:
NA.24
PubChem Substance ID:
329823535
UNSPSC Code:
41116107
EC Number:
212-726-7
MDL number:
MFCD00167245

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产品名称

林可霉素 盐酸盐 一水合物, Pharmaceutical Secondary Standard; Certified Reference Material

InChI key

LFZGYTBWUHCAKF-DCNJEFSFSA-N

InChI

1S/C18H34N2O6S.ClH.H2O/c1-5-6-10-7-11(20(3)8-10)17(25)19-12(9(2)21)16-14(23)13(22)15(24)18(26-16)27-4;;/h9-16,18,21-24H,5-8H2,1-4H3,(H,19,25);1H;1H2/t9-,10-,11+,12-,13+,14-,15-,16-,18-;;/m1../s1

SMILES string

Cl[H].[H]O[H].CCC[C@@H]1C[C@H](N(C)C1)C(=O)N[C@H]([C@@H](C)O)[C@H]2O[C@H](SC)[C@H](O)[C@@H](O)[C@H]2O

grade

certified reference material
pharmaceutical secondary standard

agency

traceable to Ph. Eur. L0650000
traceable to USP 1367005

API family

lincomycin

CofA

current certificate can be downloaded

packaging

pkg of 1 g

technique(s)

HPLC: suitable
gas chromatography (GC): suitable

application(s)

pharmaceutical (small molecule)

format

neat

storage temp.

-10 to -25°C

Quality Level

300

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Analysis Note

These secondary standards offer multi-traceability to the USP and EP primary standards, where they are available.

Application

Lincomycin Hydrochloride may be used as a pharmaceutical reference standard for the determination of the analyte in pharmaceutical formulations by various chromatography techniques.
These Secondary Standards are qualified as Certified Reference Materials. These are suitable for use in several analytical applications including but not limited to pharma release testing, pharma method development for qualitative and quantitative analyses, food and beverage quality control testing, and other calibration requirements.

General description

Pharmaceutical secondary standards for application in quality control, provide pharma laboratories and manufacturers with a convenient and cost-effective alternative to the preparation of in-house working standards.

Other Notes

This Certified Reference Material (CRM) is produced and certified in accordance with ISO 17034 and ISO/IEC 17025. All information regarding the use of this CRM can be found on the certificate of analysis.
To see an example of a Certificate of Analysis for this material enter LRAC0278 in the slot below. This is an example certificate only and may not be the lot that you receive.

pictograms

Exclamation mark
GHS07

signalword

Warning

Hazard Classifications

Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

target_organs

Respiratory system

存储类别

11 - Combustible Solids

wgk

WGK 2

flash_point_f

Not applicable

flash_point_c

Not applicable

法规信息

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Liquid chromatographic method for separation of lincomycin from its related substances.
Orwa JA, et al.
Journal of Chromatography A, 829(1-2), 161-166 (1998)
Development and validation of a gradient HPLC method for the determination of clindamycin and related compounds in a novel tablet formulation.
Platzer DJ, White BA.
Journal of Pharmaceutical and Biomedical Analysis, 41(1), 84-88 (2006)
K Vučićević-Prčetić et al.
Journal of pharmaceutical and biomedical analysis, 56(4), 736-742 (2011-08-16)
Liquid chromatography with tandem mass spectrometry (LC/MS/MS) methods for the determination of gentamicin, lincomycin and spectinomycin in the presence of their impurities were developed and tested. Chromatographic separations were achieved using gradient elution on a C18 column. All components were

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