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安全信息

41980

Supelco

1,3-二硝基苯

for HPLC derivatization, for the detection of steroids

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About This Item

线性分子式:
C6H4(NO2)2
CAS号:
99-65-0
分子量:
168.11
Beilstein:
1105654
EC 号:
202-776-8
MDL编号:
MFCD00007222
UNSPSC代码:
12164500
PubChem化学物质编号:
329756169
NACRES:
NA.21

等级

for HPLC derivatization

质量水平

100

方案

≥99.0% (HPLC)

表单

powder or crystals

质量

for the detection of steroids

沸点

297 °C (lit.)

mp

84-86 °C (lit.)
89-92 °C

密度

1.368 g/mL at 25 °C (lit.)

痕量阳离子

Ca: ≤10 mg/kg
Cd: ≤5 mg/kg
Co: ≤5 mg/kg
Cr: ≤5 mg/kg
Cu: ≤5 mg/kg
Fe: ≤5 mg/kg
K: ≤50 mg/kg
Mg: ≤5 mg/kg
Mn: ≤5 mg/kg
Na: ≤50 mg/kg
Ni: ≤5 mg/kg
Pb: ≤5 mg/kg
Zn: ≤5 mg/kg

应用

general analytical

SMILES字符串

[O-][N+](=O)c1cccc(c1)[N+]([O-])=O

InChI

1S/C6H4N2O4/c9-7(10)5-2-1-3-6(4-5)8(11)12/h1-4H

InChI key

WDCYWAQPCXBPJA-UHFFFAOYSA-N

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一般描述

1,3-Dinitrobenzene is a steam volatile, crystallizes from ethanol in the form of pale yellow rhombic-bipyramidal plates. It does not react with aqueous sodium hydroxide or sodium sulphite solution. It can be useful in manufacturing explosives, lubricants, polymerization inhibitors and corrosion inhibitors.

应用

It was used in preparing mobile phase for achiral tests to evaluate both thermodynamic and kinetic performances of the Crab-like columns in resolution of a wide range of racemates (like benzodiazepines, N-derivatized amino acids, and free carboxylic acids) both in normal phase and polar organic mode.

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警示用语：

Danger

危险分类

Acute Tox. 1 Dermal - Acute Tox. 2 Inhalation - Acute Tox. 2 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - STOT RE 2

储存分类代码

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

WGK

WGK 3

闪点(°F)

302.0 °F - closed cup

闪点(°C)

150 °C - closed cup

个人防护装备

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

法规信息

新产品

历史批次信息供参考:

分析证书(COA)

Lot/Batch Number
BCBZ5245

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Wiley-VCH
Ullmann's Fine Chemicals, 3, 140-141 (2014)
Stephen R Steiner et al.
Neurotoxicology, 32(4), 362-373 (2011-03-16)
This study demonstrated that 1,3-dinitrobenzene-induced (1,3-DNB) oxidative stress led to the oxidative carbonlyation of specific protein targets in DI TNC1 cells. 1,3-DNB-induced mitochondrial dysfunction, as indicated by loss of tetramethyl rhodamine methyl ester (TMRM) fluorescence, was initially observed at 5h
Jianfeng Zang et al.
Analytica chimica acta, 683(2), 187-191 (2010-12-21)
A sensitive electrochemical sensor has been fabricated to detect ultratrace nitroaromatic explosives using ordered mesoporous carbon (OMC). OMC was synthesized and characterized by scanning electron microscopy, transmission electron microscopy and nitrogen adsorption/desorption measurements. Glassy carbon electrodes functionalized with OMC show
Young Sook Lee et al.
Toxicology letters, 189(2), 145-151 (2009-05-30)
Several studies have shown that 1,3-dinitrobenzene (1,3-DNB) causes injury to Sertoli cells and induces apoptosis in the surrounding germinal cells in male laboratory rats; however, the mechanism by which 1,3-DNB functions is not well understood. In this study, we investigated
Yongyan Mou et al.
Journal of forensic sciences, 54(4), 846-850 (2009-05-22)
The application of attenuated total reflection (ATR)-Fourier transform infrared (FTIR) spectromicroscopy for detection of explosive particles in fingerprints is described. The combined functions of ATR-FTIR spectromicroscopy are visual searching of particles in fingerprints and measuring the FTIR spectra of the
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