等级
for GC derivatization
质量水平
检测方案
≥85.0% (T)
形式
solid
质量
LiChropur™
反应适用性
reagent type: catalyst
core: boron
reagent type: derivatization reagent
reaction type: Alkylations
技术
gas chromatography (GC): suitable
SMILES字符串
CCC[B-](CCC)(CCC)CCC.[Na+]
一般描述
Sodium tetrapropylborate (NaBPr4) belongs to the class of tetraalkylborates, which are commonly used as derivatization agents to accomplish the multielement speciation of organometallic compounds on account of their ability to react with elements such as mercury, lead and tin. NaBPr4 is preferred because it eliminates the need for organic solvents as required in Grignard reactions, also resulting in reduced analysis time.
应用
Sodium tetrapropylborate may be used as a derivatization agent to enhance the sensitivity of methylmercury in fish, organolead compounds in water and road dust samples and mercury species in sea water samples prior to their determination using microwave digestion with gas chromatography-mass spectrometry (GC-MS), GC coupled to microwave-induced plasma atomic-emission spectrometry (MIP-AES) and GC with inductively coupled plasma (ICP) MS, respectively.
法律信息
LiChropur is a trademark of Merck KGaA, Darmstadt, Germany
相关产品
产品编号
说明
价格
警示用语：
Danger
危险声明
危险分类
Pyr. Sol. 1 - Water-react 2
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
法规信息
新产品
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分析证书(COA)
Lot/Batch Number
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Mercury speciation analysis in sea water by solid phase microextraction-gas chromatography-inductively coupled plasma mass spectrometry using ethyl and propyl derivatization. Matrix effects evaluation
Bravo-Sanchez LR, et al.
Spectrochimica Acta. Part B: Atomic Spectroscopy, 59(1), 59-66 (2004)
Comparison of two derivatization reagents for the simultaneous determination of organolead and organomanganese compounds using solid-phase microextraction followed by gas chromatography with atomic emission detection
Pe?alver R, et al.
Talanta, 87(8), 268-275 (2011)
In situ propylation using sodium tetrapropylborate as a fast and simplified sample preparation for the speciation analysis of organolead compounds using GC-MIP-AES
Heisterkamp M and Adams FC
Journal of Analytical Atomic Spectrometry, 14(9), 1307-1311 (1999)
Determination of methylmercury in fish using focused microwave digestion following by Cu2+ addition, sodium tetrapropylborate derivatization, n-heptane extraction, and gas chromatography-mass spectrometry
Chen SS, et al.
Journal of Chromatography A, 1024(1-2), 209-215 (2004)
A comparison of alkyl derivatization methods for speciation of mercury based on solid phase microextraction gas chromatography with furnace atomization plasma emission spectrometry detection.
Grinberg P, et al.
Journal of Analytical Atomic Spectrometry, 18(8), 902-909 (2003)
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