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Merck
CN

16898

次乌头碱

analytical standard

别名:

16,16-trimethoxy-4-(methoxymethyl)-20-methyl-,8-acetate benzoate,(1-α,6-α,14-α,15-α,16-β)-aconitane-8,13,14,15-tetraol

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关于此项目

经验公式（希尔记法）:
C33H45NO10
化学文摘社编号:
6900-87-4
分子量:
615.71
NACRES:
NA.24
UNSPSC Code:
12352200

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InChI

1S/C33H45NO10/c1-17(35)44-33-21-19(14-31(38,28(42-6)26(33)36)27(21)43-29(37)18-10-8-7-9-11-18)32-20(40-4)12-13-30(16-39-3)15-34(2)25(32)22(33)23(41-5)24(30)32/h7-11,19-28,36,38H,12-16H2,1-6H3/t19-,20+,21?,22?,23+,24?,25?,26+,27-,28+,30+,31-,32?,33-/m1/s1

InChI key

FIDOCHXHMJHKRW-XCIBRDTCSA-N

SMILES string

O=C(C1=CC=CC=C1)O[C@H]2[C@@]3(O)[C@@H](OC)[C@H](O)[C@]4(OC(C)=O)C5[C@H](OC)C6C([C@@H](OC)CC[C@]6(CN7C)COC)(C75)[C@H](C3)C42

grade

analytical standard

assay

≥97.5% (HPLC)

optical activity

[α]/D 22.5±2.5°, c = 0.1 in chloroform

shelf life

limited shelf life, expiry date on the label

format

neat

storage temp.

2-8°C

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General description

Hypaconitine is a constituent of diester-diterpene Aconitum alkaloids (AAs), which are found in aconite plants.

Application

Hypaconitine may be used as an analytical standard for the determination of the analyte in biological samples, Aconitum tubers by liquid chromatography (LC) based techniques.

pictograms

Skull and crossbones
GHS06

signalword

Danger

Hazard Classifications

Acute Tox. 2 Inhalation - Acute Tox. 2 Oral

存储类别

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

wgk

WGK 2

flash_point_f

Not applicable

flash_point_c

Not applicable

法规信息

涉药品监管产品
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历史批次信息供参考:

分析证书(COA)

Lot/Batch Number
BCBZ6608
BCBW6149
BCBR8710

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Ying Xie et al.
Journal of chromatography. A, 1093(1-2), 195-203 (2005-10-20)
By optimizing the extraction, separation and analytical conditions, a reliable and accurate high-performance liquid chromatography (HPLC) method coupled with photodiode array detector (DAD) was developed for simultaneous quantitative determination of six Aconitum alkaloids, i.e., aconitine, mesaconitine, hypaconitine, benzoylaconine, benzoylmesaconine and
Rina Kaneko et al.
Journal of mass spectrometry : JMS, 41(6), 810-814 (2006-06-14)
The Aconitum species (Ranunculaceae) are widely distributed in northern Asia and North America. Their roots are popularly used in herbal medicines in China and Japan. Many cases of accidental, suicidal and homicidal intoxication with this plant have been reported; some
Determination of aconitine, hypaconitine and mesaconitine in urine using hollow fiber liquid-phase microextraction combined with high-performance liquid chromatography
Yang Y, et al.
Journal of Chromatography. B, Biomedical Applications, 878(28), 2811-2816 (2010)
Simultaneous determination of aconitine, mesaconitine, hypaconitine, bulleyaconitine and lappaconitine in human urine by liquid chromatography-electrospray ionization-tandem mass spectrometry
Li M and Cai Z
Analytical Methods : Advancing Methods and Applications, 5(16), 4034-4038 (2013)
Simultaneous analysis of aconitine, mesaconitine, hypaconitine, and jesaconitine in whole blood by LC-MS-MS using a new polymer column
Hattori H, et al.
Forensic Toxicology, 27(1), 7-11 (2009)
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