156272
3,5-二硝基苯甲酰氯
≥96.5%, solid
别名:
DNBC, NSC 2697
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关于此项目
线性分子式:
(O2N)2C6H3COCl
化学文摘社编号:
分子量:
230.56
NACRES:
NA.21
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
202-750-6
MDL number:
Beilstein/REAXYS Number:
990249
产品名称
3,5-二硝基苯甲酰氯, ≥96.5%
InChI key
NNOHXABAQAGKRZ-UHFFFAOYSA-N
InChI
1S/C7H3ClN2O5/c8-7(11)4-1-5(9(12)13)3-6(2-4)10(14)15/h1-3H
SMILES string
[O-][N+](=O)c1cc(cc(c1)[N+]([O-])=O)C(Cl)=O
vapor density
7.6 (vs air)
assay
≥96.5%
form
solid
bp
196 °C/11 mmHg (lit.)
mp
68-69 °C (lit.)
functional group
acyl chloride
nitro
Quality Level
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Application
3,5-二硝基苯甲酰氯可用于对吡啶中的羟基进行定量估算。 它可用于以下合成：
3,5-二硝基苯甲酰氯也可用作以下化合物的衍生剂：
- 3,5-二氨基-N-环丙基苯甲酰胺
- 3,5-二硝基-N-环丙基苯甲酰胺
- 4-（3,5-二硝基苯基）-6-（二丙-2-基氨基）-2-H-1,3,5-噻二嗪-2-硫酮
3,5-二硝基苯甲酰氯也可用作以下化合物的衍生剂：
- 发酵食品中存在的生物胺，其可通过液相色谱法（LC）进行测定
- 存在于生物体液中的多胺，其可通过高效液相色谱（HPLC）进行测定
General description
3,5-二硝基苯甲酰氯（DNBC）的晶体属于斜方晶系和Pna21空间群。 其已广泛用于醇类试剂的检测。
signalword
Danger
hcodes
Hazard Classifications
Skin Corr. 1B
存储类别
8A - Combustible corrosive hazardous materials
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges
法规信息
危险化学品
此项目有
Synthesis and characterization of aromatic poly (amides) based on 3, 5-diamino-N-cyclopropylbenzamide.
Tundidor-Camba A, et al.
Royal Society of Chemistry Advances, 5(29), 23057-23066 (2015)
Rapid Determination of Organic Hydroxyl Groups with 3, 5,-Dinitrobenzoyl Chloride.
Robinson Jr WT, et al.
Analytical Chemistry, 33(8), 1030-1034 (1961)
A Markowska et al.
Roczniki Akademii Medycznej w Bialymstoku (1995), 42(1), 129-140 (1997-01-01)
A carbocyclic analogue of distamycin was obtained, in which the N-methylpyrrole rings were substituted by disubstituted benzene rings. Additionally, N-chloro- or N-bromoacetyl groups, displaying alkylating properties, were introduced. The synthesis, starting from 3,5-dinitrobenzoyl chloride, consisted of five stages.
3, 5-Dinitrobenzoyl chloride.
Wang HY, et al.
Acta Crystallographica Section E, Structure Reports Online, 65(10), o2460-o2460 (2009)
S Wongyai et al.
Biomedical chromatography : BMC, 2(6), 254-257 (1988-11-01)
Analytical methods are described for the quantitative determination of putrescine, cadaverine, spermidine, spermine and the acetylated derivatives of spermidine and spermine in biological fluids using pre-column derivatization with either benzoyl chloride or 3,5-dinitrobenzoyl chloride, which were added to each sample
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