质量水平
产品线
Novabiochem®
检测方案
≥95.0% (acidimetric)
≥98% (TLC)
≥99.0% (HPLC)
形式
powder
反应适用性
reaction type: Boc solid-phase peptide synthesis
制造商/商品名称
Novabiochem®
mp
70-73 °C
应用
peptide synthesis
官能团
amine
储存温度
2-8°C
InChI
1S/C19H27ClN2O6/c1-19(2,3)28-18(26)22-15(16(23)24)10-6-7-11-21-17(25)27-12-13-8-4-5-9-14(13)20/h4-5,8-9,15H,6-7,10-12H2,1-3H3,(H,21,25)(H,22,26)(H,23,24)
InChI key
ATUMDPHEFWGCJF-UHFFFAOYSA-N
相关类别
一般描述
Standard building block for introduction of lysine amino-acid residues by Boc SPPS.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] K. Noda, et al. (1969) Bull. Chem. Soc. Jpn., 43, 1883.
[2] B. W. Erickson, et al. (1973) J. Am. Chem. Soc., 95, 3757.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] K. Noda, et al. (1969) Bull. Chem. Soc. Jpn., 43, 1883.
[2] B. W. Erickson, et al. (1973) J. Am. Chem. Soc., 95, 3757.
联系
Replaces: 04-12-0068
分析说明
Colour (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in DMF): -12.0 - -10.0 °
Purity (TLC(011A)): ≥ 98 %
Purity (TLC(0811)): ≥ 98 %
Assay (HPLC, area%): ≥ 99.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Solubility (1mmoll in 2ml DCM): clearly soluble
Assay (acidimetric): ≥ 95.0 %
Enantiomeric purity: ≥ 99.5 % (a/a)
To see the solvent systems used for TLC of Novabiochem® products please click here.
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in DMF): -12.0 - -10.0 °
Purity (TLC(011A)): ≥ 98 %
Purity (TLC(0811)): ≥ 98 %
Assay (HPLC, area%): ≥ 99.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Solubility (1mmoll in 2ml DCM): clearly soluble
Assay (acidimetric): ≥ 95.0 %
Enantiomeric purity: ≥ 99.5 % (a/a)
To see the solvent systems used for TLC of Novabiochem® products please click here.
法律信息
Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
法规信息
新产品
实验方案
Anhydrous HF is the preferred reagent for peptide cleavage from Boc-based resins, versatile and effective for various peptide synthesis.
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