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安全信息

B-004

Supelco

苯甲酰芽子碱标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

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About This Item

经验公式（希尔记法）:
C16H19NO4
CAS号:
519-09-5
分子量:
289.33
MDL编号:
MFCD00070263
UNSPSC代码:
41116107
PubChem化学物质编号:
329773092
NACRES:
NA.24

等级

certified reference material

质量水平

300

形式

liquid

特点

SNAP-N-SPIKE®, SNAP-N-SHOOT®

包装

ampule of 1 mL

制造商/商品名称

Cerilliant®

drug control

Narcotic Licence Schedule A (Switzerland); estupefaciente (Spain); Decreto Lei 15/93: Tabela IB (Portugal)

浓度

1.0 mg/mL in methanol

技术

gas chromatography (GC): suitable
liquid chromatography (LC): suitable

应用

forensics and toxicology

格式

single component solution

运输

wet ice

储存温度

−20°C

SMILES字符串

CN1[C@H]2CC[C@@H]1[C@H]([C@H](C2)OC(=O)c3ccccc3)C(O)=O

InChI

1S/C16H19NO4/c1-17-11-7-8-12(17)14(15(18)19)13(9-11)21-16(20)10-5-3-2-4-6-10/h2-6,11-14H,7-9H2,1H3,(H,18,19)/t11-,12+,13-,14+/m0/s1

InChI key

GVGYEFKIHJTNQZ-RFQIPJPRSA-N

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一般描述

该认证参考标准品适用于各种 LC/MS 或 GC/MS 应用，包括从法医分析和临床毒理学到尿液药物测试。

苯甲酰爱康宁是可卡因的初级代谢产物，也是确定吸食可卡因的主要生物标记物。苯甲酰爱康宁也是处方药 Esterom 中的主要药物成分，Esterom 是一种局部镇痛药，用于缓解肌肉疼痛。

应用

该认证参考溶液（CRM)也可用于以下应用：
  • 开发和确认用于测定115份收缴样品中可卡因产品的可卡因、两种主要降解产物以及常见掺杂剂的高效液相色谱-二极管阵列检测器（HPLC-DAD）方法
  • 采用整体分子印迹聚合物（MIP）固相微萃取（SPME）和之后的紫外检测分析人尿样品中的苯甲酰爱康宁
  • 通过疏水相互作用-串联质谱法（HILIC-MS/MS）分离和测定头发样品中的可卡因及其代谢产物― 苯甲酰爱康宁、芽子碱甲酯和可卡乙碱
  • 通过超高效液相色谱-串联质谱法（UHPLC-MS/MS）评估干血斑（DBS）中的可卡因、苯甲酰爱康宁、 可卡乙碱、芽子碱甲酯（EME）和去甲可卡因
  • 通过超高压液相色谱--电喷雾电离（UPLC-ESI）和三重四极杆串联质谱进行尸体血样中甲苯噻嗪、游离吗啡、6 -乙酰吗啡、可待因、可卡因和苯甲酰爱康宁的多残留分析。

特点和优势

  • 经ISO/IEC 17025 和ISO 17034认证进行全面表征
  • 随附全面的分析证书（CoA），标明稳定性、均匀性、浓度准确性、不确定性和可追溯性
  • 通过实时稳定性研究进行严格测试以确保准确性和有效期
  • 采用确认合规的精密天平以重力测定法制备，以确保最低的不确定性
  • 装入安瓿并在氩气氛围下火焰密封以确保长有效期
  • 以便捷、DEA赦免的形式提供以提高实验室效率

法律信息

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany
Snap-N-Shoot is a registered trademark of Cerilliant Corporation
Snap-N-Spike is a registered trademark of Merck KGaA, Darmstadt, Germany

相关产品

产品编号
说明
价格

B-001

苯甲酰芽子碱-d3 溶液, 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

B-007

苯甲酰芽子碱标准液 溶液, 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

B-008

苯甲酰芽子碱-d3 溶液, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

B-013

苯甲酰牙子碱-D8 溶液, 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

B-014

苯甲酰牙子碱-D8 溶液, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

C-009

Cocaethylene-D3 solution, 100 μg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

C-010

可卡乙碱 溶液, 1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

C-024

Cocaethylene-D8 solution, 100 μg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

C-088

Cocaine Multi-component Mixture solution, 250 μg/mL each component in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

H-017

m-Hydroxybenzoylecgonine solution, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

H-135

对羟基可卡因 盐酸盐 溶液, 1 mg/mL in acetonitrile (as free base), certified reference material, ampule of 1 mL, Cerilliant®

警示用语：

Danger

危险分类

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Flam. Liq. 2 - STOT SE 1

靶器官

Eyes,Central nervous system

WGK

WGK 2

闪点(°F)

closed cup

闪点(°C)

closed cup

法规信息

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分析证书(COA)

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Thomas Bouvarel et al.
Talanta, 233, 122611-122611 (2021-07-04)
A simple, selective, and sensitive method involving a miniaturized solid phase extraction step based on a monolithic molecularly imprinted polymer (MIP) directly coupled on-line to UV detection was developed for the determination of benzoylecgonine (BZE) in complex biological samples. Monolithic
Nadine Schaefer et al.
Analytical and bioanalytical chemistry, 405(1), 247-258 (2012-10-19)
In the context of driving ability diagnostics in Germany, administrative cutoffs for various drugs and pharmaceuticals in urine have been established. Two liquid chromatography-tandem mass spectrometry methods for simultaneous detection and quantification of amphetamines, designer amphetamines, benzoylecgonine, benzodiazepines, opiates, and
Sara Castiglioni et al.
Environmental science & technology, 47(3), 1452-1460 (2012-12-25)
The aim of this study was to integrally address the uncertainty associated with all the steps used to estimate community drug consumption through the chemical analysis of sewage biomarkers of illicit drugs. Uncertainty has been evaluated for sampling, chemical analysis
Charles A Dackis et al.
Journal of substance abuse treatment, 43(3), 303-312 (2012-03-02)
This is a randomized, double-blind, placebo-controlled study of modafinil treatment for cocaine dependence. Patients (N = 210) who were actively using cocaine at baseline were randomized to 8 weeks of modafinil (0 mg/day, 200 mg/day, or 400 mg/day) combined with
N Nikolettos et al.
Clinical and experimental obstetrics & gynecology, 39(1), 36-42 (2012-06-09)
To investigate the response of pregnant and non pregnant rat myometrium to benzoylecgonine, a cocaine metabolite, and oxytocin and to investigate the efficiency of ritodrine and atosiban to overcome the effects of benzoylecgonine and oxytocin. Isolation of rat myometrial tissue
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