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Merck
CN

THS09034

H-Cube® Mini continuous flow hydrogenation reactor

AC/DC input 100 / 240 V AC

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W × H × D

217 mm × 200 mm × 250 mm

weight

6.5 kg (14.33 lb)

General description

  • Hydrogen is generated through electrolysis of water
  • A continuous flow of hydrogen and solvent are passed through the reactor from ambient conditions up to 100°C and 100 bar
  • When desired parameters are achieved, solvent is changed to reactant
  • The hydrogen/compound is passed through a packed column containing solid catalyst (CatCart®), where the reaction takes place
  • The product leaves the column, but the catalyst stays behind. Reductions vary in scale from 10 mg-10 g

Specifications:
  • Temperature Range: Ambient to 100°C
  • Pressure Range: 1 bar to 100 bar
  • Flow Rate: 0.1-3 mL/min
  • Hydrogen Generation: 20-25 mL/min
  • Water Reservoir Capacity: 100 mL

Legal Information

CatCart is a registered trademark of ThalesNano Nanotechnology Inc.
H-Cube is a registered trademark of ThalesNano Nanotechnology Inc.

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Martin Pettersson et al.
Journal of medicinal chemistry, 57(3), 1046-1062 (2014-01-17)
Herein we describe the design and synthesis of a novel series of γ-secretase modulators (GSMs) that incorporates a pyridopiperazine-1,6-dione ring system. To align improved potency with favorable ADME and in vitro safety, we applied prospective physicochemical property-driven design coupled with
Continuous Flow Hydrogenation of Functionalized Pyridines.
Irfan M, Petricci E, Glasnov TN, Taddei M, Kappe OC.
Chemistry (Weinheim An Der Bergstrasse, Germany), 9, 1327-1334 (2009)
Systematic evaluation of the palladium-catalyzed hydrogenation under flow conditions.
Hattori T, Tsubone A, Sawama Y, Monguchi Y, Sajiki H.
Tetrahedron, 70(32), 4790-4798 (2014)
Flow synthesis of annulated 5-aryl-substituted pyridines by tandem intramolecular inverse-electron-demand hetero-/retro-Diels-Alder reaction.
Martin RE, Lenz M, Akzieu T, Aebi JD, Forzy L.
Tetrahedron Letters, 49, 6703-6707 (2013)
Synthesis of an azabicyclic framework towards (?)-actinophyllic acid.
Mortimer D, Whiting M, Harrity JPA, Jones S, Coldham I.
Tetrahedron Letters, 55, 1255-1257 (2014)
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