形式
liquid
质量水平
质量
Arxada quality
制造商/商品名称
Arxada AG
浓度
98.0-100.3 % (w/w) (T)
杂质
≤0.30% water
≤4.00 g/L free amine
密度
0.994 g/mL at 20 °C (lit.)
SMILES字符串
CCN(CC)C(=O)CC(C)=O
InChI
1S/C8H15NO2/c1-4-9(5-2)8(11)6-7(3)10/h4-6H2,1-3H3
InChI key
NTMXFHGYWJIAAE-UHFFFAOYSA-N
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应用
N,N-Diethylacetoacetamide is a β-dicarbonyl compound that can be used to synthesize potent calcium channel blockers such as 2,6,6-trimethyl-3-diethylaminocarbonyl-4-aryl-5-oxo-1,4,5,6,7,8-hexahydroquinoline derivatives and N,N-diethyl-2,6,6-trimethyl-4-(3-nitrophenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxamide. It can also undergo Michael addition in the presence of bis(2,4-pentanedionato)nickel(II) catalyst.
WGK
WGK 3
闪点(°F)
201.2 °F
闪点(°C)
94 °C
个人防护装备
Eyeshields, Gloves
Nickel-catalyzed Michael additions of. beta.-dicarbonyls.
Nelson JH
The Journal of Organic Chemistry, 45(7), 1246-1249 (1980)
N, N-Diethyl-2, 6, 6-trimethyl-4-(3-nitrophenyl)-5-oxo-1, 4, 5, 6, 7, 8-hexahydroquinoline-3-carboxamide.
Linden A
Acta Crystallographica Section C, Crystal Structure Communications, 58(7), 436-438 (2002)
Studies on 3-Diethyl-aminocarbonyl-1, 4; 5, 6, 7, 8-hexahydroquinoline Derivatives and their Calcium Channel Antagonistic Activities in vitro.
K?smetli E
Arzneimittelforschung, 54(07), 371-375 (2004)
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