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表单
macroporous
质量水平
反应适用性
reaction type: solution phase peptide synthesis
reactivity: imine reactive
标记范围
~2.0-3.5 mmol/g loading
粒径
20-50 mesh
mp
>300 °C (lit.)
储存温度
2-8°C
一般描述
Cyanoborohydride, polymer supported: is a polymer-supported reducing agent used in reductive amination reactions at room temperature.
应用
Polymer supported cyanoborohydride (PSCBH) has been used in the reductive alkylation aminocyclitols for the preparation of corresponding secondary amines.
It can also be used:
It can also be used:
- In combination with manganese dioxide (MnO2) for one-pot conversion of alcohols to secondary or tertiary amines.
- In the synthesis of natural products, (±)-oxomaritidine and (±)-epimaritidine.
法律信息
Amberlite is a trademark of DuPont de Nemours, Inc.
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
个人防护装备
Eyeshields, Gloves, type N95 (US)
Ley, S.V.
J. Chem. Soc., Perkin Trans., 2239-2239 (1998)
Synthesis of the alkaloids (?)-oxomaritidine and (?)-epimaritidine using an orchestrated multi-step sequence of polymer supported reagents
Ley S, et al.
Journal of the Chemical Society. Perkin Transactions 1, 3(10), 1251-1252 (1999)
Habermann, J.
J. Chem. Soc., Perkin Trans., 3127-3127 (1998)
Hutchins, R.O. et al.
Journal of the Chemical Society. Chemical Communications, 1088-1088 (1978)
Small-Scale One-Pot Reductive Alkylation of Unprotected Aminocyclitols with Supported Reagents
Sisa M, et al.
Synthesis, 2008(19), 3167-3170 (2008)
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