同位素纯度
≥99.5 atom % D
质量水平
检测方案
≥99% (CP)
形式
liquid
技术
NMR: suitable
杂质
≤0.03% water
water
折射率
n20/D 1.403 (lit.)
bp
65-66 °C (lit.)
mp
−106 °C (lit.)
密度
0.985 g/mL at 25 °C (lit.)
质量偏移
M+8
储存温度
2-8°C
SMILES字符串
[2H]C1([2H])OC([2H])([2H])C([2H])([2H])C1([2H])[2H]
InChI
1S/C4H8O/c1-2-4-5-3-1/h1-4H2/i1D2,2D2,3D2,4D2
InChI key
WYURNTSHIVDZCO-SVYQBANQSA-N
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一般描述
四氢呋喃-d8(THF-d8,TDF)是一种氘代NMR溶剂,可用于基于NMR的研究和分析。溶解在THF-d8中的甲醇和乙酸之间的质子交换速率的1H NMR线形分析已有报道。它可作为溶剂参与氘代三[双(三甲基甲硅烷基)酰胺]钍和氘代三[双(三甲基甲硅烷基)酰胺]铀的合成。15N,15N′-二戊氘苯基甲脒(DPFA)的动态NMR光谱已在THF-d8中进行了研究。
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警示用语:
Danger
危险分类
Acute Tox. 4 Oral - Carc. 2 - Eye Irrit. 2 - Flam. Liq. 2 - STOT SE 3
靶器官
Central nervous system, Respiratory system
补充剂危害
WGK
WGK 1
闪点(°F)
closed cup
闪点(°C)
closed cup
法规信息
危险化学品
美国出口管控1C298产品
Preparation and hydrogen-deuterium exchange of alkyl and hydride bis(trimethylsilyl) amido derivatives of the actinide elements.
Inorganic Chemistry, 20(9), 2991-2995 (1981)
Dynamic NMR study of the interference between cyclic proton exchange, selfassociation and hindered rotation of diphenylformamidine in tetrahydrofuran.
Berichte der Bunsengesellschaft fur physikalische Chemie, 92(4), 469-485 (1988)
NMR lineshape theory of superimposed intermolecular spin exchange reactions and its action to the system acetic acid/methanol/tetrahydrofuran-d8.
Journal of Magnetic Resonance, 36(3), 287-300 (1979)
Dalton transactions (Cambridge, England : 2003), 44(36), 16156-16163 (2015-08-22)
The synthesis and full characterization, including Nuclear Magnetic Resonance (NMR) data ((1)H, (13)C{(1)H} and (119)Sn{(1)H}), for a series of Me3SnX (X = O-2,6-(t)Bu2C6H3 (), (Me3Sn)N(2,6-(i)Pr2C6H3) (), NH-2,4,6-(t)Bu3C6H2 (), N(SiMe3)2 (), NEt2, C5Me5 (), Cl, Br, I, and SnMe3) compounds in
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