398985
N-甲基-1,2-苯二胺
97%
别名:
1-N-甲基苯-1,2-二胺, 2(甲氨基)苯胺, 2-N-甲基苯-1,2-二胺, 2-氨基-N-甲基苯胺, N-甲基-1,2-二氨基苯, N-甲基-1,2-苯二胺, N-甲基邻二氨基苯, N-甲基邻苯二胺, N1-甲基-1,2-苯二胺
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关于此项目
线性分子式:
CH3NHC6H4NH2
化学文摘社编号:
分子量:
122.17
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
225-297-6
MDL number:
产品名称
N-甲基-1,2-苯二胺, 97%
InChI key
RPKCLSMBVQLWIN-UHFFFAOYSA-N
InChI
1S/C7H10N2/c1-9-7-5-3-2-4-6(7)8/h2-5,9H,8H2,1H3
SMILES string
CNc1ccccc1N
assay
97%
form
liquid
refractive index
n20/D 1.612 (lit.)
bp
123-124 °C/10 mmHg (lit.)
mp
22 °C (lit.)
density
1.075 g/mL at 25 °C (lit.)
functional group
amine
Quality Level
Application
N -甲基-1,2-苯二胺可用于以下研究：
- 一锅法合成 1-甲基-2-（杂）芳基苯并咪唑。
- 1-甲基-1 H -苯并咪唑-2（3 H ）-硫酮的制备。
- 血管紧张素 II 受体拮抗剂替米沙坦的全合成。
- 烯酮二硫代缩醛制备苯并咪唑类。
General description
N-甲基-1,2-苯二胺是一种 邻位 -二胺。N-甲基-1，2-苯二胺的原位生成重氮化阳离子曾用于玻碳电极的电化学修饰。
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Warning
Hazard Classifications
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Irrit. 2 - Skin Irrit. 2
存储类别
10 - Combustible liquids
wgk
WGK 3
flash_point_f
235.4 °F - closed cup
flash_point_c
113 °C - closed cup
ppe
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
此项目有
Hizbullah Khan et al.
Acta crystallographica. Section E, Structure reports online, 64(Pt 6), o1141-o1141 (2008-01-01)
The title compound, C(8)H(8)N(2)S, was prepared by the condensation of N-methyl-1,2-phenyl-enediamine and carbon disulfide. The crystal structure is stabilized by a C-H⋯π inter-action between a benzene H atom and the benzene ring of a neighbouring mol-ecule, and by inter-molecular N-H⋯S
Recent developments in use of heteropolyacids, their salts and polyoxometalates in organic synthesis.
Heravi MM and Sadjadi S.
Journal of the Iranian Chemical Society, 6(1), 1-54 (2009)
Synthesis, 1273-1273 (1992)
A Sanjeev Kumar et al.
Beilstein journal of organic chemistry, 6, 25-25 (2010-05-27)
An efficient synthesis of the angiotensin II receptor antagonist Telmisartan (1) is presented involving a cross coupling of 4-formylphenylboronic acid 10 with 2-(2-bromophenyl)-4,4-dimethyl-2-oxazoline (11) as the key step (90% yield). The benzimidazole moiety 15 was constructed regioselectively via a reductive
Tony Breton et al.
Langmuir : the ACS journal of surfaces and colloids, 24(16), 8711-8718 (2008-07-26)
The electrochemically induced functionalization of glassy carbon electrode by aryl groups having an aliphatic amine group was achieved by reduction of in situ generated diazonium cations in aqueous media. The corresponding diazonium cations of 4-aminobenzylamine, 2-aminobenzylamine, 4-(2-aminoethyl)aniline, N-methyl-1,2-phenylenediamine, and N
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