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About This Item
经验公式（希尔记法）:
C16H13ClO2
CAS号:
分子量:
272.73
MDL编号:
UNSPSC代码:
12352005
PubChem化学物质编号:
NACRES:
NA.22
推荐产品
等级
for chiral derivatization
质量水平
蒸汽密度
2 (vs air)
蒸汽压
180 mmHg ( 20 °C)
表单
liquid
浓度
18 mM in acetone
折射率
n20/D 1.3602
密度
0.79 g/mL at 25 °C
官能团
chloro
储存温度
2-8°C
SMILES字符串
ClC(=O)OC(C1c2c(cccc2)c3c1cccc3)C
InChI
1S/C16H13ClO2/c1-10(19-16(17)18)15-13-8-4-2-6-11(13)12-7-3-5-9-14(12)15/h2-10,15H,1H3
InChI key
SFRVOKMRHPQYGE-UHFFFAOYSA-N
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一般描述
（+）-1-（9-芴基）乙基氯甲酸酯是高度荧光的化合物 1，通常用作手性衍生剂，用在进行反相 HPLC 分析之前分离外消旋体。
应用
- β-甲基氨基丙氨酸（BMAA）对映体的手性分析：详细介绍了氯甲酸(+)-1--9-芴基乙酯（FLEC）的衍生化和随后的LC-MS/MS分析，增进了我们对氨基酸′立体化学的理解 （Zurita et al., 2019）。
- DL-氨基酸的对映选择性胶束电动色谱：利用氯甲酸(+)-1--9-芴基乙酯进行衍生化，结合UV诱导的荧光检测进行氨基酸的分析，改善了分析方法（Prior et al., 2018）。
警示用语：
Danger
危险声明
危险分类
Eye Dam. 1 - Flam. Liq. 2 - STOT SE 3
靶器官
Central nervous system
补充剂危害
储存分类代码
3 - Flammable liquids
WGK
WGK 3
闪点(°F)
1.4 °F
闪点(°C)
-17 °C
法规信息
危险化学品
易制毒化学品（3类）
Reversed-phase high-performance liquid chromatographic analysis of atenolol enantiomers in plasma after chiral derivatization with (+)-1-(9-fluorenyl) ethyl chloroformate.
Rosseel MT, et al.
Journal of Chromatography. B, Biomedical Applications, 568(1), 239-245 (1991)
K C Chan et al.
Electrophoresis, 16(4), 504-509 (1995-04-01)
Direct enantiomeric separations of some racemic amino acids derivatized with 9-fluorenylmethyl chloroformate were obtained using cyclodextrin-modified micellar electrokinetic chromatography (CD/MEKC) with a buffer made up of 5 mM sodium borate (pH 9.2), 150 mM sodium dodecyl sulfate (SDS) and 40
M T Rosseel et al.
Journal of chromatography, 568(1), 239-245 (1991-07-17)
A sensitive high-performance liquid chromatographic method for the determination of the enantiomers of atenolol in rat plasma has been developed. Racemic atenolol and practolol (internal standard) were extracted from alkalinized plasma (pH 12) into dichloromethane containing 3% (v/v) heptafluoro-1-butanol, and
Radu-Cristian Moldovan et al.
Journal of chromatography. A, 1467, 400-408 (2016-08-25)
In the context of bioanalytical method development, process automatization is nowadays a necessity in order to save time, improve method reliability and reduce costs. For the first time, a fully automatized micellar electrokinetic chromatography-mass spectrometry (MEKC-MS) method with in-capillary derivatization
J Sukbuntherng et al.
Journal of analytical toxicology, 19(3), 139-147 (1995-05-01)
To study the disposition kinetics of methamphetamine (MAP), we have developed a sensitive high-performance liquid chromatographic (HPLC) assay to quantitate the enantiomers of MAP and its major metabolites, amphetamine (AP), p-hydroxymethamphetamine (p-OH-MAP), and p-hydroxyamphetamine (p-OH-AP), the latter two of which
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