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质量水平
方案
98%
表单
liquid
折射率
n20/D 1.622 (lit.)
沸点
125-126 °C/19 mmHg (lit.)
溶解性
alcohol: miscible(lit.)
chloroform: miscible(lit.)
diethyl ether: miscible(lit.)
water: insoluble(lit.)
密度
1.799 g/mL at 25 °C (lit.)
官能团
iodo
SMILES字符串
COc1ccccc1I
InChI
1S/C7H7IO/c1-9-7-5-3-2-4-6(7)8/h2-5H,1H3
InChI key
DVQWNQBEUKXONL-UHFFFAOYSA-N
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一般描述
在含有 L-脯氨酸和 L-乳酸阴离子和非手性季铵阳离子的手性离子液体存在下，2-碘苯甲醚参与 2,3-二氢呋喃的钯催化对映选择性 Heck 芳基化反应。
应用
2-碘茴香醚已用于钯/铜催化的邻-（1-炔基）茴香醚的合成。
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
235.4 °F - closed cup
闪点(°C)
113 °C - closed cup
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
Adam Morel et al.
Dalton transactions (Cambridge, England : 2003), 42(4), 1215-1222 (2012-11-09)
Chiral ionic liquids (CILs) containing L-prolinate and L-lactate anions and non-chiral quaternary ammonium cations were employed in the palladium catalyzed enantioselective Heck arylation of 2,3-dihydrofuran with aryl iodides (iodobenzene, 4-iodotoluene, 2-iodoanisole, 4-iodoanisole, 4-iodoacetophenone). In all the reactions 2-aryl-2,3-dihydrofuran (3) was
Dawei Yue et al.
The Journal of organic chemistry, 70(25), 10292-10296 (2005-12-06)
[reaction: see text] 2,3-Disubstituted benzo[b]furans are readily prepared under very mild reaction conditions by the palladium/copper-catalyzed cross-coupling of various o-iodoanisoles and terminal alkynes, followed by electrophilic cyclization with I2, PhSeCl, or p-O2NC6H4SCl. Aryl- and vinylic-substituted alkynes undergo electrophilic cyclization in
Naoyuki Yasaka et al.
Analytical sciences : the international journal of the Japan Society for Analytical Chemistry, 34(10), 1183-1188 (2018-10-12)
Aryl halides are a very important category of compounds that include many vital drugs and key industrial additives, such as clofibrate and bromobenzene, respectively. Due to their importance, our research group previously developed a novel fluorescence labeling approach for their
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