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方案
98%
表单
liquid
折射率
n20/D 1.523 (lit.)
沸点
97 °C/11 mmHg (lit.)
mp
6.5-7 °C (lit.)
密度
1.27 g/mL at 25 °C (lit.)
SMILES字符串
Cc1c(F)cccc1[N+]([O-])=O
InChI
1S/C7H6FNO2/c1-5-6(8)3-2-4-7(5)9(10)11/h2-4H,1H3
InChI key
GXPIVRKDWZKIKZ-UHFFFAOYSA-N
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一般描述
2-Fluoro-6-nitrotoluene undergoes reduction in the presence of stannous chloride, followed by benzoylation to yield N-(3-fluoro-o-tolyl)benzamide. 2-Fluoro-6-nitrotoluene undergoes reaction with concentrated nitric acid at 100°C to yield 2-fluoro-6-nitrobenzoic acid.
应用
2-Fluoro-6-nitrotoluene has been used in the preparation of 4-fluoroindole via Leimgruber-Batcho procedure.
警示用语：
Warning
危险分类
Acute Tox. 4 Oral - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
192.2 °F - closed cup
闪点(°C)
89 °C - closed cup
个人防护装备
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
139. Heterocyclic fluorine compounds. Part IV. Monofluoroindazoles.
Barben IK and Suschitzky H.
Journal of the Chemical Society, 672-676 (1960)
A synthesis of (-)-indolactam V.
Semmelhack MF and Rhee H.
Tetrahedron Letters, 34(9), 1395-1398 (1993)
359. Preparation of some fluoronitro-and aminofluoro-benzoic acids, and of fluoronitro-benzenes,-toluenes, and-xylenes.
Valkanas G and Hopff H.
Journal of the Chemical Society, 1925-1927 (1963)
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