检测方案
98%
形式
liquid
折射率
n20/D 1.523 (lit.)
bp
97 °C/11 mmHg (lit.)
mp
6.5-7 °C (lit.)
密度
1.27 g/mL at 25 °C (lit.)
SMILES字符串
Cc1c(F)cccc1[N+]([O-])=O
InChI
1S/C7H6FNO2/c1-5-6(8)3-2-4-7(5)9(10)11/h2-4H,1H3
InChI key
GXPIVRKDWZKIKZ-UHFFFAOYSA-N
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一般描述
2-Fluoro-6-nitrotoluene undergoes reduction in the presence of stannous chloride, followed by benzoylation to yield N-(3-fluoro-o-tolyl)benzamide. 2-Fluoro-6-nitrotoluene undergoes reaction with concentrated nitric acid at 100°C to yield 2-fluoro-6-nitrobenzoic acid.
应用
2-Fluoro-6-nitrotoluene has been used in the preparation of 4-fluoroindole via Leimgruber-Batcho procedure.
警示用语：
Warning
危险分类
Acute Tox. 4 Oral - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
WGK
WGK 3
闪点(°F)
192.2 °F
闪点(°C)
89 °C
个人防护装备
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
359. Preparation of some fluoronitro-and aminofluoro-benzoic acids, and of fluoronitro-benzenes,-toluenes, and-xylenes.
Valkanas G and Hopff H.
Journal of the Chemical Society, 1925-1927 (1963)
A synthesis of (-)-indolactam V.
Semmelhack MF and Rhee H.
Tetrahedron Letters, 34(9), 1395-1398 (1993)
139. Heterocyclic fluorine compounds. Part IV. Monofluoroindazoles.
Barben IK and Suschitzky H.
Journal of the Chemical Society, 672-676 (1960)
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