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质量水平
检测方案
98%
旋光性
[α]23/D −18°, c = 2 in carbon tetrachloride
光学纯度
ee: 99% (GLC)
mp
71-73 °C (lit.)
储存温度
2-8°C
SMILES字符串
CC1(C)[C@@]2(C)CC[C@@]1(OC2=O)C(Cl)=O
InChI
1S/C10H13ClO3/c1-8(2)9(3)4-5-10(8,6(11)12)14-7(9)13/h4-5H2,1-3H3/t9-,10+/m0/s1
InChI key
PAXWODJTHKJQDZ-VHSXEESVSA-N
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一般描述
(1S)-(-)-氯代樟脑酸是一种手性衍生剂,可通过(-)-(1S,4R)-樟脑酸与氯化亚砜反应制备。
警示用语:
Danger
危险声明
危险分类
Skin Corr. 1B
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
个人防护装备
Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges
(-)-(1S, 4R)-Camphanoyl Chloride.
Organic Syntheses, 71, 48-48 (1993)
Chiral separations of ?-blocking drug substances using derivatization with chiral reagents and normal-phase high-performance liquid chromatography.
Journal of Chromatography A, 636(2), 231-241 (1993)
The determination of the absolute configurations of diastereomers of (S)-camphanoyl 3-hydroxy-5-oxohexanoic acid derivatives by X-ray crystallography.
Angewandte Chemie (International ed. in English), 41(7), 1198-1202 (2002-12-20)
Journal of chromatography, 491(2), 355-366 (1989-07-21)
A reversed-phase high-performance liquid chromatographic assay has been developed for determination of (R)-(--)-and (S)-(+)-proxyphylline in human plasma. The procedure is based on liquid-solid extraction of proxyphylline from plasma followed by derivatization of extracted proxyphylline with (--)-camphanoyl chloride. The ratio between
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