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方案
97%
表单
powder
折射率
n20/D 1.521 (lit.)
沸点
158 °C/742 mmHg (lit.)
密度
1.07 g/mL at 25 °C (lit.)
SMILES字符串
Cc1ncsc1C
InChI
1S/C5H7NS/c1-4-5(2)7-3-6-4/h3H,1-2H3
InChI key
UWSONZCNXUSTKW-UHFFFAOYSA-N
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一般描述
Radical bromination of 4,5-dimethylthiazole using N-bromosuccinimide in the presence of 2,2′-azobisisobutyronitrile yields mono-, tri- and tetrabromo compounds.
应用
4,5-Dimethylthiazole was used in the preparation of 4-(bromomethyl)-5-(dibromomethyl)thiazole.
警示用语：
Danger
危险分类
Acute Tox. 4 Oral - Eye Dam. 1 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
储存分类代码
3 - Flammable liquids
WGK
WGK 3
闪点(°F)
123.8 °F - closed cup
闪点(°C)
51 °C - closed cup
法规信息
新产品
Mouaffak Al Hariri et al.
The Journal of organic chemistry, 62(2), 405-410 (1997-01-24)
4-(Bromomethyl)-5-(dibromomethyl)thiazole (1) was prepared in good yields by bromination of 4,5-dimethylthiazole with 3.3 equiv of NBS in the presence of AIBN. Treatment of 1 with sodium iodide led to a thiazole o-quinodimethane 2 which was trapped in situ with dienophiles
Selective Bromination of 4, 5-Dimethylthiazole with N-Bromosuccinimide.
Al Hariri M, et al.
European Journal of Organic Chemistry, 1998(4), 593-594 (1998)
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