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方案
97%
表单
liquid
折射率
n20/D 1.551 (lit.)
沸点
214 °C (lit.)
密度
1.37 g/mL at 25 °C (lit.)
官能团
bromo
SMILES字符串
Cc1ccc(Br)c(C)c1
InChI
1S/C8H9Br/c1-6-3-4-8(9)7(2)5-6/h3-5H,1-2H3
InChI key
YSFLQVNTBBUKEA-UHFFFAOYSA-N
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一般描述
Gold-catalyzed coupling reaction of pyrazine with 1-bromo-2,4-dimethylbenzene has been reported. 1-Bromo-2,4-dimethylbenzene reacts with Mg and DMF, followed by the reaction with I2 and aq.NH3 to afford the corresponding aromatic nitrile.
警示用语：
Warning
危险声明
危险分类
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
174.2 °F - closed cup
闪点(°C)
79 °C - closed cup
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
Gold (I)-catalyzed direct C-H arylation of pyrazine and pyridine with aryl bromides.
Li M and Hua R.
Tetrahedron Letters, 50(13), 1478-1481 (2009)
Transformation of aromatic bromides into aromatic nitriles via formations of grignard reagents and their DMF adducts.
Ishii G, et al.
Tetrahedron Letters, 52(18), 2404-2406 (2011)
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