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方案
≥97%
mp
90-94 °C (lit.)
溶解性
acetone: soluble 74.4 g/100ml at 20 °C(lit.)
benzene: soluble 44.4 g /100ml at 20 °C(lit.)
dioxane: soluble 65.6 g/100ml at 20 °C(lit.)
hexane: soluble 0.4 g/100ml at 20 °C(lit.)
isopropanol: soluble 21 g/100ml at 20 °C(lit.)
官能团
chloro
sulfone
SMILES字符串
Clc1ccc(cc1)S(=O)(=O)c2ccccc2
InChI
1S/C12H9ClO2S/c13-10-6-8-12(9-7-10)16(14,15)11-4-2-1-3-5-11/h1-9H
InChI key
OFCFYWOKHPOXKF-UHFFFAOYSA-N
一般描述
4-Chlorophenyl phenyl sulfone is also referred to as sulphenone. It participates in palladium-catalyzed amidation reaction in the presence of low CO pressures and an iodide salt.
应用
4-Chlorophenyl phenyl sulfone was employed in polyetherification reaction of 4,4′-dihalodiphenyl sulfones.
警示用语：
Warning
危险分类
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
个人防护装备
dust mask type N95 (US), Eyeshields, Gloves
Robert J. Perry et al.
The Journal of organic chemistry, 61(21), 7482-7485 (1996-10-18)
The palladium-catalyzed amidation of electron-deficient aryl chlorides proceeds readily in the presence of low CO pressures and a slight excess of an iodide salt. The rates of amidation are accelerated over those without added salt, and iodide is preferred over
Reductive dehalogenation versus substitution in the polyetherification of 4, 4'-dihalodiphenyl sulfones with bisphenolates.
Percec V, et al.
Macromolecules, 26(14), 3650-3662 (1993)
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