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质量水平
方案
95%
折射率
n20/D 1.452 (lit.)
沸点
102-104 °C/11 mmHg (lit.)
密度
1.054 g/mL at 25 °C (lit.)
官能团
ester
ketone
SMILES字符串
CCOC(=O)C1CCCC1=O
InChI
1S/C8H12O3/c1-2-11-8(10)6-4-3-5-7(6)9/h6H,2-5H2,1H3
InChI key
JHZPNBKZPAWCJD-UHFFFAOYSA-N
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一般描述
本文研究了 2-氧代环戊烷甲酸乙酯与溴苄在微型反应器中的相转移苄基化反应 。2-氧代环戊烷甲酸乙酯参与伯醇和仲醇的钴 (II) Schiff 碱络合物催化氧化 。
应用
2-氧代环戊烷甲酸乙酯用于 (±)- 顺，顺 -螺 [4.4] 壬烷-1,6-二醇的立体选择性合成 。也用于合成 tanikolide 。
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
170.6 °F - closed cup
闪点(°C)
77 °C - closed cup
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
Masaharu Ueno et al.
Chemical communications (Cambridge, England), (8)(8), 936-937 (2003-05-15)
Phase-transfer alkylation in a microreactor proceeds smoothly, and the reaction has been found to be more efficient than that in a round-bottomed flask with vigorous stirring; we have observed by an optical microscope study that an interfacial area provided by
An improved synthesis and resolution of (?)-< i> cis, cis</i>-spiro [4.4] nonane-1, 6-diol.
Nieman JA, et al.
Tetrahedron Asymmetry, 4(9), 1973-1976 (1993)
A new synthesis of tanikolide.
Zhai H, et al.
Tetrahedron Letters, 44(14), 2893-2894 (2003)
Cobalt (II) Schiff's base complex catalysed oxidation of alcohols with dioxygen in the presence of ethyl 2-oxocyclopentanecarboxylate.
Punniyamurthy T and Iqbal J.
Tetrahedron Letters, 35(23), 4007-4010 (1994)
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