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线性分子式:
NH2COOC(CH3)3
化学文摘社编号:
分子量:
117.15
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
224-209-3
Beilstein/REAXYS Number:
1744500
MDL number:
产品名称
氨基甲酸叔丁酯, 98%
InChI key
LFKDJXLFVYVEFG-UHFFFAOYSA-N
InChI
1S/C5H11NO2/c1-5(2,3)8-4(6)7/h1-3H3,(H2,6,7)
SMILES string
CC(C)(C)OC(N)=O
assay
98%
form
solid
mp
105-108 °C (lit.)
functional group
amine
Quality Level
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Application
氨基甲酸叔丁酯被用于 N-Boc保护的苯胺钯催化合成。它被用于合成四取代吡咯,在C-3位以酯或酮基官能化。
General description
氨基甲酸 叔丁酯与各种芳基(Het)卤化物的钯催化交叉偶联反应已被研究,其中Cs2CO3 作为1,4-二恶烷(溶剂)中的碱。
存储类别
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
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The Journal of organic chemistry, 74(12), 4634-4637 (2009-06-13)
The scope of Pd-catalyzed synthesis of N-Boc-protected anilines from aryl bromides and commercially available tert-butyl carbamate is described. For the first time, this process can be conducted at room temperature (17-22 degrees C) using a combination of Pd(2)dba(3).CHCl(3) and a
One-Pot Three-Component Synthesis of Tetrasubstituted NH Pyrroles from Secondary Propargylic Alcohols, 1, 3-Dicarbonyl Compounds and tert-Butyl Carbamate.
Cadierno V, et al.
Journal of Heterocyclic Chemistry, 47(1), 233-236 (2010)
Pd-catalyzed amidation of aryl (Het) halides with< i> tert</i>-butyl carbamate.
Qin L, et al.
Tetrahedron Letters, 51(33), 4446-4448 (2010)
Zeljko M Svedružić et al.
PloS one, 7(3), e32293-e32293 (2012-04-06)
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