质量水平
检测方案
98%
形式
liquid
折射率
n20/D 1.545 (lit.)
bp
195-196 °C (lit.)
密度
1.123 g/mL at 25 °C (lit.)
SMILES字符串
COc1ccccc1Cl
InChI
1S/C7H7ClO/c1-9-7-5-3-2-4-6(7)8/h2-5H,1H3
InChI key
QGRPVMLBTFGQDQ-UHFFFAOYSA-N
一般描述
2-Chloroanisole undergoes acetylation with acetic anhydride over large pore zeolites to give 4-acetyl-2-chloroanisole.
应用
2-Chloroanisole was used in headspace solid-phase microextraction method for the determination of haloanisoles in wine and spirit samples.
WGK
WGK 3
闪点(°F)
168.8 °F
闪点(°C)
76 °C
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
Keith Smith et al.
Organic & biomolecular chemistry, 1(9), 1560-1564 (2003-08-21)
The acetylation of aryl ethers using acetic anhydride in the presence of zeolites under modest conditions in a solvent-free system gave the corresponding para-acetylated products in high yields. The zeolite can be recovered, regenerated and reused to give almost the
Natalia Campillo et al.
Journal of chromatography. A, 1210(2), 222-228 (2008-10-18)
A headspace solid-phase microextraction (HS-SPME) method for the determination of 12 haloanisoles in wine and spirit samples using gas chromatography with atomic emission detection (GC-AED) was developed. The different factors affecting the efficiency of the extraction were carefully optimized. The
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