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质量水平
方案
98%
表单
liquid
折射率
n20/D 1.536 (lit.)
沸点
193 °C (lit.)
密度
1.164 g/mL at 25 °C (lit.)
官能团
chloro
SMILES字符串
COc1cccc(Cl)c1
InChI
1S/C7H7ClO/c1-9-7-4-2-3-6(8)5-7/h2-5H,1H3
InChI key
YUKILTJWFRTXGB-UHFFFAOYSA-N
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一般描述
One-step preparation of 3-chloroanisole from the corresponding 3-substituted nitrobenzene has been reported.
应用
3-Chloroanisole was employed as starting reagent in the regioselective synthesis of 4- and 7-alkoxyindoles. It was also employed as electrolyte additive for the overcharging protection of Li-ion cell.
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
163.4 °F - closed cup
闪点(°C)
73 °C - closed cup
个人防护装备
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
One-step preparation of some 3-substituted anisoles.
Zilberman J.
Organic Process Research & Development, 7(3), 303-305 (2003)
3-Chloroanisole for overcharge protection of a Li-ion cell.
Lee Y-G and Cho J.
Electrochimica Acta, 52(25), 7404-7408 (2007)
Roberto Sanz et al.
The Journal of organic chemistry, 72(14), 5113-5118 (2007-06-15)
An efficient and regioselective synthesis of 4- and 7-alkoxyindoles has been developed from commercially available starting materials such as 3-halophenols and 3-chloroanisole. Directed ortho-metalation followed by two palladium-catalyzed processes, a Sonogashira coupling and a tandem amination/cyclization reaction, allows the synthesis
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