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质量水平
方案
97%
表单
liquid
折射率
n20/D 1.488 (lit.)
沸点
74 °C/15 mmHg (lit.)
mp
3-5 °C (lit.)
密度
0.980 g/mL at 20 °C
0.971 g/mL at 25 °C (lit.)
官能团
ketone
储存温度
2-8°C
SMILES字符串
CC1=CC(=O)CC1
InChI
1S/C6H8O/c1-5-2-3-6(7)4-5/h4H,2-3H2,1H3
InChI key
CHCCBPDEADMNCI-UHFFFAOYSA-N
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一般描述
3-Methyl-2-cyclopentenone undergoes reduction in presence of triethylammonium formate and palladium catalyst to form saturated ketone. It undergoes B(C6F5)3 catalyzed hydrosilation to yield complex reaction mixtures of 1,2 addition products and oligomers.
应用
3-Methyl-2-cyclopentenone was used in the synthesis of 2-hydroxy-3-methyl-2-cyclopentenone.
储存分类代码
10 - Combustible liquids
WGK
WGK 3
闪点(°F)
149.0 °F - closed cup
闪点(°C)
65 °C - closed cup
个人防护装备
Eyeshields, Gloves, multi-purpose combination respirator cartridge (US)
A new synthesis of cyclopentenones: dihydrojasmone.
Hendrickson JB and Palumbo PS.
The Journal of Organic Chemistry, 50(12), 2110-2112 (1985)
B(C6F5)3 catalyzed hydrosilation of enones and silyl enol ethers.
Blackwell JM, et al.
Tetrahedron, 58(41), 8247-8254 (2002)
Palladium-catalyzed reductions of. alpha.,. beta.-unsaturated carbonyl compounds, conjugated dienes, and acetylenes with trialkylammonium formates.
Cortese NA and Heck NA.
The Journal of Organic Chemistry, 43(20), 3985-3987 (1978)
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